arXiv · 1604.00601
Calibration of higher eigenmodes of cantilevers
Abstract
A method is presented for calibrating the higher eigenmodes (resonance modes) of atomic force microscopy cantilevers that can be performed prior to any tip-sample interaction. The method leverages recent efforts in accurately calibrating the first eigenmode by providing the higher-mode stiffness as a ratio to the first mode stiffness. A one-time calibration routine must be performed for every cantilever type to determine the power-law relationship between stiffness and frequency, which is then stored for future use on similar cantilevers. Then, future calibrations only require a measurement of the ratio of resonance frequencies and the stiffness of the first mode. This method is verified through stiffness measurements using three independent approaches: interferometric measurement, AC approach-curve calibration, and finite element analysis simulation. Power-law values for calibrating higher-mode stiffnesses are reported for three popular multifrequency cantilevers. Once the higher-mode stiffnesses are known, the amplitude of each mode can also be calibrated from the thermal spectrum by application of the equipartition theorem.
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Aleksander Labuda, Marta Kocun, Tim Walsh, Jieh Meinhold, Tania Proksch, Waiman Meinhold, Martin Lysy, Roger Proksch. 2016-04-03. Calibration of higher eigenmodes of cantilevers. https://doi.org/10.1063/1.4955122
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