SearcharxivSearch

arXiv · 2012.10830

Undulating compression and multi-stage relaxation in a granular column consisting of dust particles or glass beads

Abstract

For fundamentally characterizing the effect of hierarchical structure in granular matter, a set of compression-relaxation tests for dust particles and glass beads confined in a cylindrical cell was performed. Typical diameter of both grains is approximately 1~mm. However, dust particles are produced by binding tiny ($\sim 5$~{\textmu}m) glass beads. The granular columns were compressed with a piston until reaching a maximum load force of 20~N with a constant compression rate $v$ ($0.17 \leq v \leq 2000$~{\textmu}m~s$^{-1}$). After that, the piston was stopped and the relaxation process was quantified. From the experimental results, we found that the compression force $F$ nonlinearly increases with the increase of compression stroke $z$ depending on particles. Besides, periodic undulation and sudden force drops were observed on $F(z)$ in dust particles and glass beads, respectively. The relaxation process was characterized by an exponential decay of stress followed by a logarithmic dependence one in both kinds of particles. These experimental findings are the main point in this study. To understand the underlying physics governing the compression mechanics, we assumed empirical forms of $F(z)$; $F\propto z^{\alpha}$ for dust particles and $F \propto \exp(z/z_G)$ for glass beads ($\alpha=2.4$ and $z_G=70$~{\textmu}m). Then, we found that the growing manners of periodic undulation and force drops were identical to those of mean compression forces, i.e., power law in dust particles and exponential in glass beads. In addition, the undulation amplitude and wavelength decreased as $v$ increased in dust-particles compression. On the basis of experimental results and the difference between dust particles and glass beads, we also discuss the origin of undulation and the physical meaning of granular-compression models used in engineering fields.

Explore related subjects

Keep this discovery

BibTeXRIS

Felipe Pacheco-Vázquez, Tomomi Omura, Hiroaki Katsuragi. 2020-12-20. Undulating compression and multi-stage relaxation in a granular column consisting of dust particles or glass beads. https://doi.org/10.1103/physrevresearch.3.013190

Cite the original work for its findings. Save a collection to share your selection of sources.

KEEP EXPLORING

Related papers

Slow Dynamics and the Geometry of Jammed Packings

Saddle points in the energy landscape of granular packings dominate the discrete steepest descent dynamics and ultimately determine the path that an out of mechanical equilibrium packing will follow and the resulting stable minimum that it will find. The saddle points that ultimately determine the resulting minima tend to be low-index saddle points. For models with an analytic energy landscape, such as the $p$-spin model, the steepest descent minimization path is affected by higher-index saddle points, which pull the system towards saddle points of decreasing index before arriving at the minima. Here, we examine the steepest descent minimization path of granular packings and compare them to the $p$-spin model. We show that the granular packing steepest descent minimization paths act like their smooth energy landscape counterparts and get attracted by saddle points. The index versus time curves for all models follow a shifted, stretched exponential. We further show that the shape parameter for the granular packings is unchanged when the energy landscape is modified to become analytic (Gaussian potential in a harmonic well) or non-local (Mari-Krzakala-Kurchan). The $p$-spin, on the other hand, has a significantly larger shape parameter. The reason is not due to the dimensionality, packing fraction, nonanalyticity, or the locality of the Hamiltonian of the models. The exact reason for the discrepancy in the shape parameter is \st{still} an unsolved mystery.

cond-mat.soft

A Phase-Field Study of Desiccation Crack Pattern Maturation under Drying-Wetting Cycles

The characteristic intersection angle of the desiccation crack relaxes from near \ang{90} toward \ang{120} under repeated drying--wetting cycles. However, the theoretical understanding of this relaxation is insufficient, especially the modeling of the drying--wetting cycles. Here we introduce a phase-field model of desiccation fracture, extending the model proposed in previous studies by adding crack healing and a scar effect left by past cracks. By repeating drying--wetting cycles in a finite element simulation, we find that the angle distribution develops a growing peak near \ang{120} as the cycle number increases, consistent with experiments. The standard deviation of the intersection angle from \ang{120} relaxes exponentially with a characteristic time of about 2.85 cycles. These results are consistent with experiments, except that the characteristic time is slightly smaller than the experimental value. Crack energy dominates the total energy and also relaxes exponentially with nearly the same characteristic cycle as the angle relaxation. This decay is driven mainly by a shortening of the effective crack length rather than a change in effective fracture toughness.

cond-mat.soft

Kinetics of ferritin crystal formation and melting in acoustically levitated droplets

Understanding protein crystallization pathways is essential for controlling crystallization in structural biology, materials science, and pharmaceutical applications. Classical nucleation theory does not fully capture crystallization processes for several proteins, including ferritin. Here, we combine acoustic levitation with small- and wide-angle X-ray scattering (SAXS and WAXS) to monitor ferritin crystallization in evaporating aqueous polyethylene glycol (PEG) solutions. Acoustic levitation rapidly drives the droplets through a broad range of protein and polymer concentrations, enabling time-resolved measurements of crystallization during evaporation. The scattering data show that ferritin crystals form during evaporation and subsequently lose their crystalline order upon further dehydration. Varying the PEG molecular weight switches between distinct crystallization pathways: one dominated by attractive protein-protein interactions and another dominated by repulsive interactions and excluded-volume effects. Furthermore, we find that lower molecular weight PEG (1000 g/mol) suppresses the dehydration-induced loss of crystalline order observed for higher molecular weight PEG (6000 g/mol), providing a simple strategy for improving protein crystal stability.

cond-mat.soft