Data for the green synthesis of exceptional braided, helical carbon nanotubes and nano spiral platelets made directly from CO$_2$

Abstract

This article describes base-line data used in conjunction with the Materials Today Chemistry article: The green synthesis of exceptional braided, helical carbon nanotubes and nano spiral platelets made directly from CO$_2$. The data includes Raman, XRD, SEM, TEM, EDX and high contrast TEM of conventional carbon nanotubes (CNTs) synthesized from carbon dioxide electrolytic splitting in molten electrolyte for comparison to synthesized helical carbon nanotubes grown in the main article. This data article also presents SEM showing that uncontrolled electrolytic CO$_2$ splitting leads to bent and deformed CNTs, rather than straight or helical CNTs, and SEM that helical carbon nanotubes and helical carbon nanoplatelets can be produced with only partial control of the electrolysis current and with no defect inducing agents. A novel, cheap synthesis of high purity helical nanocarbon is discovered. A baseline and comparative experimental data for non-helical analogues is presented. Both the non-helical and helical nanocarbon are synthesized from the greenhouse gas CO$_2$ by molten carbonate electrolysis.