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A Widdowson

Publications and source records attributed to A Widdowson.

2 recordsLinked to original sources

D retention and material defects probed using Raman microscopy in JET limiter samples and beryllium-based synthesized samples

We report on the detection by means of Raman spectroscopy of amorphous beryllium deuteride, BeD 2 , in magnetron sputtered deposits synthesized in two different laboratories and containing about 20 at.% of deuterium. In contrast, this signature has not been found for the JET limiter samples studied coming from the inner, outer or upper limiters, even when coming from a deposition zone of the limiters. We give a way to disentangle that BeD 2 signature from other signatures falling in the same spectroscopic range and mainly related to other phenomena. We also analyze the Raman characteristics of the JET sample defects. These results could help in the interpretation of D thermal desorption spectra and in future analyses of JET thick Be deposit divertor tiles.

physics.chem-ph

Surface analysis of tiles and samples exposed to the first JET campaigns with the ITER-Like Wall

This paper reports on the first post-mortem analyses of tiles removed from JET after the first campaigns with the ITER-like Wall (ILW) during 2011-2 [1]. Tiles from the divertor have been analysed by the Ion Beam Analysis (IBA) techniques Rutherford Backscattering Spectroscopy (RBS) and Nuclear Reaction Analysis (NRA) and by Secondary Ion Mass Spectrometry (SIMS) to determine the amount of beryllium deposition and deuterium retention in the tiles exposed to the scrape-off layer. Films 10-20 microns thick were present at the top of Tile 1, but only very thin films (<1 micron) were found in the shadowed areas and on other divertor tiles. The total amount of Be found in the divertor following the ILW campaign was a factor of ~9 less that the material deposited in the 2007-9 carbon campaign, after allowing for the longer operations in 2007-9.

physics.ins-det