SearcharxivSearch

arXiv subjects

Bryan Roebuck

Publications and source records attributed to Bryan Roebuck.

2 recordsLinked to original sources

Direct current thermo-mechanical testing: Principles, uncertainty hierarchy, and its role in advanced materials characterisation

Direct current thermo-mechanical testing (DC-TMT), based on resistive Joule heating, enables rapid heating and cooling, steep thermal gradients and simultaneous mechanical loading, making it a powerful tool for probing deformation, phase transformations, oxidation-assisted damage and creep under conditions inaccessible to conventional furnace-based methods. Despite its growing use, DC-TMT lacks formal standardisation and is often misinterpreted as equivalent to bulk isothermal testing, overlooking intrinsic differences in thermal and mechanical fields. This review addresses that gap by consolidating four decades of research on specimen geometry, temperature measurement, strain characterisation and environmental control, and by classifying uncertainty sources as dominant, secondary and conditional. Evidence from modelling and experiment shows that temperature gradients, heating rate and gauge representativeness govern the reliability of inferred material behaviour. Applications across aluminium, steels, nickel-based superalloys, titanium alloys, hardmetals, zirconium alloys, shape memory alloys and additively manufactured systems are critically assessed. The review highlights domains where DC-TMT provides reproducible mechanistic insight and conditions where direct equivalence with bulk data is not warranted. Implications include the need for transparent reporting, multi-sensor temperature validation and integration with electro-thermal modelling to enable rigorous, mechanism-focused interpretation.

cond-mat.mtrl-sci

Ultra high-temperature deformation in a single crystal superalloy: Meso-scale process simulation and micro-mechanisms

A mesoscale study of a single crystal nickel-base superalloy subjected to an industrially relevant process simulation has revealed the complex interplay between microstructural development and the micromechanical behaviour. As sample gauge volumes were smaller than the length scale of the highly cored structure of the parent material from which they were produced, their subtle composition differences gave rise to differing work hardening rates, influenced by varying secondary dendrite arm spacings, gamma-prime phase solvus temperatures and a topologically inverted gamma/gamma-prime microstructure. The gamma-prime precipitates possessed a characteristic `X' morphology, resulting from the simultaneously active solute transport mechanisms of thermally favoured octodendritic growth and N-type rafting, indicating creep-type mechanisms were prevalent. High resolution-electron backscatter diffraction (HR-EBSD) characterisation reveals deformation patterning that follows the gamma/gamma-prime microstructure, with high geometrically necessary dislocation density fields localised to the gamma/gamma-prime interfaces; Orowan looping is evidently the mechanism that mediated plasticity. Examination of the residual elastic stresses indicated the `X' gamma-prime precipitate morphology had significantly enhanced the deformation heterogeneity, resulting in stress states within the gamma channels that favour slip, and that encourage further growth of gamma-prime precipitate protrusions. The combination of such localised plasticity and residual stresses are considered to be critical in the formation of the recrystallisation defect in subsequent post-casting homogenisation heat treatments.

cond-mat.mtrl-sci