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Chithra Karunakaran

Publications and source records attributed to Chithra Karunakaran.

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Investigating the Limits of Hard X-ray Coherence Length Measurement Employing Young's Double Slit Experiment

Young's double slit experiment has been the most explored technique to gauge the coherence properties of a given system. The limits of this technique in characterizing spatial coherence properties of high emittance, hard x-ray synchrotron sources have been performed at the BXDS-IVU beamline, Canadian Light Source (CLS). High emittance synchrotron sources have always been assumed to possess sub-optimal coherence properties, especially in the hard X-ray regime. While this is largely true, it is very important to understand the limits of coherence for these existing high emittance sources. We have demonstrated that the Young's double slit experiment has harsher limits than what is normally expected in the form of inherent ambiguity. We present data obtained at multiple energies in both the horizontal and vertical direction leading to a thorough understanding of the fundamental limitations of employing Young's double slit experiment to characterize inherently low coherence length systems. We have put forth a novel numerical technique to estimate the source size directly from the Young's double slit interference patterns. With these results, we have demonstrated that CLS has functional coherent beam properties in the hard X-ray regime with Spatial coherence lengths ranging from 5.37$\mu \text{m}$ to 17.61$\mu \text{m}$ in the horizontal direction. The same in the vertical direction was at least 3 times larger. Finally, we present theoretical calculations showcasing the limits of Young's double slit experiment in characterizing diffraction limited sources.

physics.optics

Cryo scanning transmission X-ray microscope optimized for spectrotomography

A cryo scanning transmission X-ray microscope, the cryo-STXM, has been designed and commissioned at the Canadian Light Source synchrotron. The instrument is designed to operate from 100 - 4000 eV (lambda = 12.4 - 0.31 nm). Users can insert a previously frozen sample, through a load lock, and rotate it plus minus 70 degrees in the beam to collect tomographic data sets. The sample can be maintained for extended periods at 92 K primarily to suppress radiation damage, and a pressure on the order of 10-9 Torr to suppress sample contamination. The achieved spatial resolution (30 nm) and spectral resolution (0.1 eV) are similar to other current soft X-ray STXMs, as demonstrated by measurements on known samples and test patterns. The data acquisition efficiency is significantly more favorable for both imaging and tomography. 2D images, 3D tomograms and 4D chemical maps of automotive hydrogen fuel cell thin sections are presented to demonstrate current performance and new capabilities, namely cryo-spectrotomography in the soft X-ray region.

physics.ins-det