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E. Mistretta

Publications and source records attributed to E. Mistretta.

3 recordsLinked to original sources

Insitu X Ray Photoemission Study of Nb Surface Under Plasma Cleaning During MID T BAKING For SRF Cavities

Specific heat treatments applied to superconducting radiofrequency (SRF) cavities, such as nitrogen infusion or Mid T baking, aim to improve the quality factor (Qo) at medium accelerating fields (10 to 20 MV/m). These treatments reduce the BCS surface resistance by tuning the mean free path of niobium over a few hundred na-nometers, either by diffusing oxygen from the native oxide layer or by diffusing nitrogen after the dissolution of the oxide layer. However, these treatments preclude the usual chemical polishing, as it would reverse the beneficial effects of the heat treatments, making the cavities highly sensitive to surface contamination. In particular, the formation of niobium carbides, which can mask the expected benefits, strongly depends on the annealing conditions, surface preparation, and the materials history. To better understand these phenomena, niobium samples was annealed under ultrahigh vacuum (Mid T baking) with Ar/O2 plasma treatment to investi-gate surface contamination with insitu heat treatment at 500 C and XPS analysis.

physics.acc-ph

Improvement of Heat-Treated Niobium Surface by In-situ Plasma Treatment Applied to Superconducting RF Resonator

A specific heat treatment at 300 C, named medium-temperature baking (Mid-T baking) is applied to superconducting radio-frequency (SRF) accelerating cavities to improve the quality factor (Qo) at medium accelerating fields (10 to 20 MV/m). This treatment is very successful when done properly as it can reduce by almost a factor of two the power dissipations in this field range. However, surface contamination can lead to the degradation of Qo instead. Plasma-based surface treatment provides an effective approach to eliminate contaminants from the Niobium surface. In this study an insitu plasma cleaning process with argon containing 10 % O2 was performed to remove hydrocarbons from Niobium surface. The treatment was applied before and after a heat treatment at 500 C under ultra-high vacuum conditions (Mid-T baking). Changes in chemical speciation and oxide layer alteration induced by plasma processing were analyzed using insitu X-ray photoelectron spectroscopy (XPS) and exsitu scanning electron microscopy (SEM). The results show that plasma treatment modifies the composition of Niobium oxides, converting a Nb2O5 layer into NbO2. Furthermore, a plasma treatment before Mid-T baking helps reduce unstable oxides such as NbxO and significantly increases the proportion of metallic Niobium at the surface. The Niobium sample treated by plasma prior to Mid-T baking showed a 53 % reduction in carbide formation. Moreover, the C1s component attributed to NbC bonds shifts toward lower binding energy, indicating the formation of a more metallic NbC phase. Whereas without plasma treatment, the higher binding energy component observed after Mid T baking is consistent with Nb2C.

physics.acc-ph

PHIL photoinjector test line

LAL is now equiped with its own platform for photoinjectors tests and Research and Developement, named PHIL (PHotoInjectors at LAL). This facility has two main purposes: push the limits of the photoinjectors performances working on both the design and the associated technology and provide a low energy (MeV) short pulses (ps) electron beam for the interested users. Another very important goal of this machine will be to provide an opportunity to form accelerator physics students, working in a high technology environment. To achieve this goal a test line was realised equipped with an RF source, magnets and beam diagnostics. In this article we will desrcibe the PHIL beamline and its characteristics together with the description of the first two photoinjector realised in LAL and tested: the ALPHAX and the PHIN RF Guns.

physics.acc-ph