arXiv subjects

G. Giunchi

Publications and source records attributed to G. Giunchi.

18 recordsLinked to original sources

arXiv2017

Carrier Transport in Magnesium Diboride: Role of Nano-inclusions

Anisotropic-gap and two-band effects smear out the superconducting transition (Tc) in literature reported thermal conductivity of MgB2, where large electronic contributions also suppress anomaly-manifestation in their negligible phononic-parts. Present thermal transport results on scarcely explored specimens featuring nano-inclusions exhibit a small but clear Tc-signature, traced to relatively appreciable phononic conduction, and its dominant electronic-scattering. The self-formed MgO as extended defects strongly scatter the charge carriers and minutely the phonons with their longer-mean-free-path near Tc. Conversely, near room temperature, the shorter-dominant-wavelength phonon's transport is hugely affected by these nanoparticles, undergoing ballistic to diffusive crossover and eventually entering the Ioffe-Regel mobility threshold regime.

cond-mat.supr-con↗

arXiv2013

Microwave Response of Coaxial Cavities Made of Bulk Magnesium Diboride

We report on the microwave (mw) properties of coaxial cavities built by using bulk MgB2 superconductor prepared by reactive liquid Mg infiltration technology. We have assembled a homogeneous cavity, by using an outer MgB2 cylinder and an inner MgB2 rod, and a hybrid cavity by using an outer copper cylinder and the same MgB2 rod as inner conductor. By the analysis of the resonance curves, in the different resonant modes, we have determined the microwave surface resistance, Rs, of the MgB2 materials as a function of the temperature and the frequency, in the absence of DC magnetic fields. At T = 4.2 K and f = 2.5 GHz, by a mw pulsed technique, we have determined the quality factor of the homogeneous cavity as a function of the input power up to a maximum level of about 40 dBm (corresponding to a maximum peak magnetic field of about 100 Oe). Contrary to what occurs in many films, Rs of the MgB2 material used does not exhibit visible variations up to an input power level of about 10 dBm and varies less than a factor of 2 on further increasing the input power of 30 dB.

cond-mat.supr-con↗

arXiv2007

Microwave response of a cylindrical cavity made of bulk MgB2 superconductor

We report on the microwave properties of a resonant cylindrical cavity made of bulk MgB2 superconductor, produced by the reactive liquid Mg infiltration process. The frequency response of the cavity has been measured in the range 5-13GHz. Among the various modes, the TE011, resonating at 9.79GHz, exhibits the highest quality factor. For this mode, we have determined the temperature dependence of the quality factor, obtaining values of the order of 10^5 in the temperature range 4.2-30K. The values of the surface resistance deduced from the measurements of the quality factor agree quite well with those independently measured in a small sample of MgB2 extracted from the same specimen from which the cavity has been obtained.

cond-mat.supr-con↗

arXiv2007

Superconducting Microwave Cavity Made of Bulk MgB2

We report the successful manufacture and characterization of a microwave resonant cylindrical cavity made of bulk MgB2 superconductor (Tc = 38.5 K), which has been produced by the Reactive Liquid Mg Infiltration technique. The quality factor of the cavity for the TE011 mode, resonating at 9.79 GHz, has been measured as a function of the temperature. At T = 4.2 K, the unloaded quality factor is 2.2x10^5; it remains of the order of 10^5 up to T ~ 30 K. We discuss the potential performance improvements of microwave cavities built from bulk MgB2 materials produced by reactive liquid Mg infiltration.

cond-mat.supr-con↗

arXiv2006

Effects of Weak Links in the Nonlinear Microwave Response of MgB2 Superconductor

We report experimental results of second-harmonic (SH) response at microwave frequency in several ceramic MgB2 samples, prepared by different methods. The SH signal has been investigated as a function of the temperature and DC magnetic field. The investigation has been carried out at low magnetic fields, where nonlinear processes arising from motion of Abrikosov fluxons are ineffective. We show that the low-temperature SH emission is ascribable to processes involving weak links. Comparison among the peculiarities of the SH signal radiated by the different samples shows that the presence of weak links strongly depends on the sample preparation method, as well as the purity and morphology of the components used for the preparation.

cond-mat.supr-con↗

arXiv2006

Near-Tc second-harmonic emission in high-density bulk MgB2 at microwave frequency

We discuss the microwave second-harmonic generation in high-density bulk MgB2, prepared by the reactive liquid Mg infiltration technology. The intensity of the harmonic signal has been investigated as a function of temperature and amplitudes of the DC and microwave magnetic fields. The results are discussed in the framework of a phenomenological theory, based on the two-fluid model, which assumes that both the microwave and static magnetic fields, penetrating in the surface layers of the sample, weakly perturb the partial concentrations of the normal and superconducting fluids. We show that, in order to account for the experimental results, it is essential to suppose that in MgB2 the densities of the normal and condensed fluids linearly depend on the temperature.

cond-mat.supr-con↗

arXiv2006

Microwave Harmonic Emission in MgB2 Superconductor: Comparison with YBaCuO

We report results of microwave second-harmonic generation in ceramic samples of MgB2, prepared by different methods. The SH signal has been investigated as a function of the temperature and the static magnetic field. The results are discussed in the framework of models reported in the literature. We show that the peculiarities of the SH signal are related to the specific properties of the sample. A comparison with the results obtained in ceramic and crystalline YBa(2)Cu(3)O(7) shows that the second-harmonic emission in MgB2 is weaker than that observed in ceramic YBa(2)Cu(3)O(7).

cond-mat.supr-con↗

arXiv2005

Microwave response of bulk MgB2 samples of different granularity

The microwave response of three high-density bulk MgB2 samples has been investigated in the linear and nonlinear regimes. The three samples, characterized by different mean size of grains, have been obtained by reactive infiltration of liquid Mg in powdered B preforms. The linear response has been studied by measuring the microwave surface impedance; the nonlinear response by detecting the power radiated by the sample at the second-harmonic frequency of the driving field. Our results suggest that bulk MgB2 prepared by the liquid Mg infiltration technique is particularly promising for manufacturing resonant cavities operating at microwave frequencies.

cond-mat.supr-con↗

arXiv2004

Surface-Barrier Effects in the Microwave Second-Harmonic Response of Superconductors in the Mixed State

We report on transient effects in the microwave second-order response of different type of superconductors in the mixed state. The samples have contemporarily been exposed to a dc magnetic field, varying with a constant rate of 60 Oe/s, and a pulsed microwave magnetic field. The time evolution of the signal radiated at the second-harmonic frequency of the driving field has been measured for about 500 s from the instant in which the dc-field sweep has been stopped, with sampling time of about 0.3 s. We show that the second-harmonic signal exhibits two relaxation regimes; an initial exponential decay, which endures roughly 10 s, and a logarithmic decay in the time scale of minutes. Evidence is given that the decay in the time scale of minutes is ruled by magnetic relaxation over the surface barrier.

cond-mat.supr-con↗

arXiv2003

Fluxon dynamics by microwave surface resistance measurements in MgB2

Field-induced variations of the microwave surface resistance, Rs(H), have been investigated in high-density ceramic MgB2. At low temperatures, several peculiarities of the Rs(H) curves cannot be justified in the framework of models reported in the literature. We suggest that they are ascribable to the unconventional vortex structure in MgB2, related to the presence of two gaps. On the contrary, the results near Tc can be accounted for by the Coffey and Clem model, with fluxons moving in the flux-flow regime, provided that the anisotropy of the upper critical field is taken into due account.

cond-mat.supr-con↗

arXiv2002

Superconducting Properties of Highly Dense MgB2 Bulk Materials

Highly dense MgB2 policrystalline bulk materials, obtained by reactive liquid infiltration, have been characterized in their superconducting transport and magnetic properties in magnetic field and in a temperature range of interest for the MgB2 compound. The products have a granular morphology of composite nature and their overall density affects their properties. The irreversibility line, Bc1(T) values, magnetically measured current densities and the trapped magnetic field are evaluated by susceptibility curves and hysteresis curves, both obtained by SQUID magnetometry for samples of different density, up to 35K and up to 5T applied magnetic field. The experimental results have been compared with the best values reported in the literature for other bulk sintering techniques.

cond-mat.supr-con↗

arXiv2002

Vortex dynamics and pinning properties analysis of MgB2 bulk samples by ac susceptibility measurements

The flux lines dynamics have been investigated on MgB2 bulk superconductors obtained by reactive liquid infiltration by measuring the ac magnetic susceptibility. The fundamental and third harmonics have been studied as a function of temperature, dc magnetic field, ac field amplitude and frequency. In order to determine the dynamical regimes governing the vortex motion, the experimental results have been compared with susceptibility curves obtained by numerical calculations of the non-linear diffusion equation for the magnetic field. The frequency behaviour of the third harmonic response, that cannot be explained by frequency dependent critical state models, has been related to the current dependence of the flux creep activation energy U(J) in the diffusion coefficient. In this way we have shown that the measured curves are correctly interpreted within the framework of a vortex glass description.

cond-mat.supr-con↗

arXiv2002

High performance new MgB2 superconducting hollow wires

MgB2 hollow wires have been produced with a new technique which uses a conventional wire manufacturing process but is applied to composite billets containing the elemental B and Mg precursors in an appropriate shape. The technique has been applied to the manufacture of both monofilamentary and multifilamentary wires of several tens meters length. The superconducting transport properties of the MgB2 hollow wires have been measured in magnetic field and in the temperature range from 4.2 to 30 K. Promising results are obtained, which indicate the possibility of application of these wires as superconductors in the temperature range of 15-30 K and at medium-high values of magnetic field.

cond-mat.supr-con↗

arXiv2001

Electrodynamic response of MgB2 sintered pellets and thin films

We present a study of the electrodynamic response of MgB2 pellets and thin film samples exhibiting critical temperatures ranging between 26 and 38 K. We have performed accurate measurements of the surface impedance ZS =RS+iXS as a function of the temperature and of the magnitude of the electromagnetic field. The temperature variation and the field dependence of ZS was measured by a dielectric resonator cavity technique in the microwave region. In particular, the temperature variation of the magnetic penetration depth was also determined in the RF region by a single coil mutual inductance method. In the case of the films, for T<TC/2 a clear exponential behavior of the penetration depth is observed, which can be explained by a simple BCS s-wave model with a reduced value of the energy gap. On the contrary, pellets show no evidence of saturation, and the experimental results strictly follow a quadratic dependence down to the lowest temperatures. This behavior can be induced by the presence of metallic Mg inclusions that may locally depress the gap. The analysis of the field dependence of the surface impedance in the microwave region confirms that the electrodynamic response of MgB2 is dominated by different sources of dissipation, depending on the sample history, likely to be ascribed to the predominance of grain boundaries or normal regions on its surface.

cond-mat.supr-con↗

arXiv2001

Temperature and junction-type dependency of Andreev reflection in MgB2

We studied the voltage and temperature dependency of the dynamic conductance of normal metal-MgB2 junctions obtained either with the point-contact technique (with Au and Pt tips) or by making Ag-paint spots on the surface of high-quality single-crystal-like MgB2 samples. The fit of the conductance curves with the generalized BTK model gives evidence of pure s-wave gap symmetry. The temperature dependency of the gap, measured in Ag-paint junctions (dirty limit), follows the standard BCS curve with 2Delta/kTc = 3.3. In out-of-plane, high-pressure point contacts we obtained almost ideal Andreev reflection characteristics showing a single small s-wave gap Delta = 2.6 +/- 0.2 (clean limit). These results support the two-gap model of superconductivity, the presence of a modified layer at the surface of the crystals and an important and non-conventional role of the impurities in MgB2.

cond-mat.supr-con↗

arXiv2001

Josephson effect in MgB_2 break junctions

We present the first observation of the DC and AC Josephson effect in MgB_2 break junctions. The junctions, obtained at 4.2 K in high-quality, high-density polycrystalline metallic MgB_2 samples, show a non-hysteretic DC Josephson effect. By irradiating the junctions with microwaves we observe clear Shapiro steps spaced by the ideal $ΔV$ value. The temperature dependence of the DC Josephson current and the dependence of the height of the steps on the microwave power are obtained. These results are a direct prove for the existence of pairs with charge 2e in this new metallic superconductor and give evidence of the superconductor-normal metal-superconductor weak link character of these junctions.

cond-mat.supr-con↗

arXiv2001

A search for incipient lattice instabilities in MgB$_{2}$ by anelastic spectroscopy

We measured the complex dynamic elastic modulus of MgB2 between 1.3 and 650 K at frequencies included between 5 and 70 kHz. The main purpose of this work is to search for possible lattice instabilities, which could contribute to enhance the electron-phonon coupling. The Young's modulus indeed presents an anomalous softening on cooling below 400 K, and hysteresis between cooling and heating. Such anomalies, however, can be accounted for by intense relaxation processes with maxima between 50 and 150 K, whose nature is not yet clarified, and by geometric defects generated by the anisotropic thermal expansion between the grains during thermal cycling. Additional intense relaxation processes are observed above room temperature, and their possible origin is discussed. The influence of the highly anharmonic in-plane vibration modes of the B atoms on the elastic and anelastic properties of MgB2 is discussed in detail.

cond-mat.supr-con↗

arXiv2001

Critical state analysis in MgB2 bulk by means of quantitative MO technique

An extended magneto-optical (MO) analysis of samples cut from high-density pellets of MgB2 is reported. For sake of comparison some magnetic measurements and critical values are also shown. Notwithstanding the fact that the optical and SEM images exhibit grains with different shape and size, all the samples investigated by MO analysis (three specimens of different shape and size) enter as a whole into a critical state. The current at different temperatures and fields, in a phase zone accessible to MO are calculated by means of a quantitative analysis. The analysis, based on the inversion of the Biot-Savart law, corresponds to three regimes: under-critical, critical and over-critical, respectively. A possible qualitative interpretation of the absence of magnetic granularity is given in the framework of a critical state likely reached by a network of strongly coupled Josephson Junctions.

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