arXiv subjects

Henning Friis Poulsen

Publications and source records attributed to Henning Friis Poulsen.

24 records · Page 2Linked to original sources

arXiv2018

X-ray coherent diffraction imaging with an objective lens: towards 3D mapping of thick polycrystals

We report on a new x-ray imaging method, which combines the high spatial resolution of coherent diffraction imaging with the ability of dark field microscopy to map grains within thick polycrystalline specimens. An x-ray objective serves to isolate a grain and avoid overlap of diffraction spots. Iterative oversampling routines are used to reconstruct the shape and strain field within the grain from the far field intensity pattern. The limitation on resolution caused by the finite numerical aperture of the objective is overcome by the Fourier synthesis of several diffraction patterns. We demonstrate the method by an experimental study of a ~500 nm Pt grain for the two cases of a real and a virtual image plane. In the latter case the spatial resolution is 13 nm rms. Our results confirm that no information on the pupil function of the lens is required and that lens aberrations are not critical.

physics.ins-det↗

arXiv2018

Imbibition in plant seeds

We describe imbibition in real and artificial plant seeds, using a combination of experiments and theory. In both systems, our experiments demonstrate that liquid permeates the substrate at a rate which decreases gradually over time. Tomographic imaging of soy seeds is used to confirmed this by observation of the permeating liquid using an iodine stain. To rationalize the experimental data, we propose a model based on capillary action which predicts the temporal evolution of the radius of the wet front and the seed mass. The depth of the wetting front initially evolves as $t^{1/2}$ in accord with the Lucas-Washburn law. At later times, when the sphere is almost completely filled, the front radius scales as $(1-t/t_{\text{max}})^{1/2}$ where $t_{\text{max}}$ is the time required to complete imbibition. The data obtained on both natural and artificial seeds collapse onto a single curve that agrees well with our model, suggesting that capillary phenomena contribute to moisture uptake in soy seeds.

physics.bio-ph↗

arXiv2016

Extended formalism for simulating compound refractive lens-based x-ray microscopes

We present a comprehensive formalism for the simulation and optimisation of CRLs in both condensing and full-field imaging configurations. The approach extends ray transfer matrix analysis to account for x-ray attenuation by the lens material. Closed analytical expressions for critical imaging parameters such as numerical aperture, vignetting, chromatic aberration and focal length are provided for both thin- and thick-lens imaging geometries.

physics.optics↗

arXiv2015

Noise Robustness of a Combined Phase Retrieval and Reconstruction Method for Phase-Contrast Tomography

Classical reconstruction methods for phase-contrast tomography consist of two stages: phase retrieval and tomographic reconstruction. A novel algebraic method combining the two was suggested by Kostenko et al. (Opt. Express, 21, 12185, 2013) and preliminary results demonstrating improved reconstruction compared to a two-stage method given. Using simulated free-space propagation experiments with a single sample-detector distance, we thoroughly compare the novel method with the two-stage method to address limitations of the preliminary results. We demonstrate that the novel method is substantially more robust towards noise; our simulations point to a possible reduction in counting times by an order of magnitude.

math.NA↗

arXiv2015

Full-field hard x-ray microscopy with interdigitated silicon lenses

Full-field x-ray microscopy using x-ray objectives has become a mainstay of the biological and materials sciences. However, the inefficiency of existing objectives at x-ray energies above 15 keV has limited the technique to weakly absorbing or two-dimensional (2D) samples. Here, we show that significant gains in numerical aperture and spatial resolution may be possible at hard x-ray energies by using silicon-based optics comprising 'interdigitated' refractive silicon lenslets that alternate their focus between the horizontal and vertical directions. By capitalizing on the nano-manufacturing processes available to silicon, we show that it is possible to overcome the inherent inefficiencies of silicon-based optics and interdigitated geometries. As a proof-of-concept of Si-based interdigitated objectives, we demonstrate a prototype interdigitated lens with a resolution of ~255 nm at 17 keV.

physics.optics↗

arXiv2015

Generalized balanced power diagrams for 3D representations of polycrystals

Characterizing the grain structure of polycrystalline material is an important task in material science. The present paper introduces the concept of generalized balanced power diagrams as a concise alternative to voxelated mappings. Here, each grain is represented by (measured approximations of) its center-of-mass position, its volume and, if available, by its second-order moments (in the non-equiaxed case). Such parameters may be obtained from 3D x-ray diffraction. As the exact global optimum of our model results from the solution of a suitable linear program it can be computed quite efficiently. Based on verified real-world measurements we show that from the few parameters per grain (3, respectively 6 in 2D and 4, respectively 10 in 3D) we obtain excellent representations of both equiaxed and non-equiaxed structures. Hence our approach seems to capture the physical principles governing the forming of such polycrystals in the underlying process quite well.

cond-mat.mtrl-sci↗