arXiv subjects

I. Snigireva

Publications and source records attributed to I. Snigireva.

5 recordsLinked to original sources

arXiv2019

X-ray scattering characterization of iron oxide nanoparticles Langmuir film on water surface and on a solid substrate

In the present study we compare a structure of a Langmuir film assembled from magnetic iron oxide nanoparticles on water surface and a structure of the same film after its transfer to a solid substrate by the Langmuir-Schaefer method. In contrast to most of related studies, where different techniques are used to characterize the films before and after the deposition, we use the same combination of X-ray reflectometry and Grazing Incidence Small-Angle X-ray scattering. In both cases -- on a liquid and on a solid substrate -- the film was identified as a well-ordered monolayer of the nanoparticles laterally organized in a two-dimensional hexagonal lattice. However parameters of the lattice were found to be slightly different depending on the type of the substrate. It is also demonstrated that Langmuir-Schaefer technique is the right way for deposition of such kind of the particles on a solid substrate.

cond-mat.soft↗

arXiv2019

Self-assembly of a binary mixture of iron oxide nanoparticles in Langmuir film: X-ray scattering study

In present study we exploited Langmuir technique to produce self-assembled arrays composed of monodisperse iron oxide nanoparticles 10 nm and 20 nm in diameter and of their binary mixture. A combination of in-situ X-ray reflectometry and Grazing-incident small-Angle X-ray scattering was used to obtain in-plane and out-of-plane structure of the arrays directly on the water surface. Surface pressure isotherms and X-ray reflectometry analysis showed that monodisperse 10 nm nanoparticles form a highly ordered monolayer, while 20 nm particles pack in three-dimensional clusters with a short-range (nearest-neighbor) correlations between the particles. In a binary mixture of 10 nm and 20 nm nanoparticles composed in proportion 3:1 the self-assembly process results in a structure where the monolayer of 10 nm particles is perturbed by the larger particles. Non-trivial mixing causes an enlargement of interparticle distance but keeps the symmetry of two-dimensional lattice of smaller nanoparticles. Estimation of the acting interactions and micromagnetic simulation suggest the optimal formation for monodisperse and binary ensembles.

cond-mat.soft↗

arXiv2019

Polarized neutron reflectometry study from iron oxide nanoparticles monolayer

We report on the polarized neutron reflectometry investigation of monolayer of magnetic iron oxide nanoparticles assembled by the Langmuir-Schaefer method. After deposition onto a solid substrate the polarized neutron reflectometry measurements in the external magnetic field were carried out. Thickness, density, roughness and in-depth resolved magnetization profile of the resulted layer were obtained from accurate fitting routine.

cond-mat.mes-hall↗

arXiv2005

Study of Optical Properties of X-ray System Based on Two Zone Plates

We presents the results of study of focusing and imaging properties of double-lens system for hard x-ray radiation consisting of two Fresnel zone plates (ZP) made from silicon. We demonstrate for the first time the phenomenon of focusing by two crystal ZP located at significant distance from each other. We investigate by both theoretically and experimentally the peculiarities of intensity distribution at the focal plane during a scan by second ZP normally to the optical axis of the system. We investigate as well the intensity distribution along the optical axis for our double-lens system from crystal ZP. We realize experimentally a registration of the focused image of the object by means of double-lens system based on ZP. Measurements are performed on the beam line BM-5 of the European Synchrotron Radiation Facility (ESRF) at the x-ray energy 9.4 keV. We elaborate a computer program for theoretical simulation of the optical properties of x-ray double-lens system based on ZPs. A calculation is made by convolution of transmission function and Kirchhoff propagator in paraxial approximation by means of Fast Fourier Transformation.

physics.optics↗

arXiv2005

High efficiency and low absorption Fresnel compound zone plates for hard X-ray focusing

Circular and linear zone plates have been fabricated on the surface of silicon crystals for the energy of 8 keV by electron beam lithography and deep ion plasma etching methods. Various variants of compound zone plates with first, second, third diffraction orders have been made. The zone relief height is about 10 mkm, the outermost zone width of the zone plate is 0.4 mkm. The experimental testing of the zone plates has been conducted on SPring-8 and ESRF synchrotron radiation sources. A focused spot size and diffraction efficiency measured by knife-edge scanning are accordingly 0.5 mkm and 39% for the first order circular zone plate.

cs.OH↗