arXiv subjects

Jakob Schwiedrzik

Publications and source records attributed to Jakob Schwiedrzik.

5 recordsLinked to original sources

arXiv2025

Filling a gap in materials mechanics: Nanoindentation at high constant strain rates upto $10^5 s^{-1}$

A central focus in high strain rate research is understanding the dynamic behavior of materials at strain rates where a strength upturn is observed. While strength upturns at strain rates of $10^3$ to $10^4~\mathrm{s}^{-1}$ have been widely reported in the literature, their occurrence in certain materials remains controversial, and the underlying physics driving this phenomenon is not yet fully understood. Current mechanical testing methods are limited, as no single technique spans the full strain rate range of $10^1$ to $10^5~\mathrm{s}^{-1}$ where this phenomenon is expected, and a unified technique would enable consistent post-deformation characterization with minimal error. To address this, we developed a customized piezoelectric in situ nanomechanical test setup, enabling constant indentation strain rates up to $10^5~\mathrm{s}^{-1}$ for the first time. Using this system, we examined rate-dependent hardness in single-crystalline molybdenum, nanocrystalline nickel, and amorphous fused silica over strain rates from $10^1$ to $10^5~\mathrm{s}^{-1}$, remarkably revealing a hardness upturn in all three materials. Further, post-deformation analysis of single-crystalline molybdenum revealed that the hardness upturn was primarily driven by increased dislocation density, with phonon drag -- traditionally considered a dominant contributor -- playing a minimal role.

cond-mat.mtrl-sci↗

arXiv2025

Resolving Discrepancies in Wood Micromechanics: Strain-Mapped Compression of Tracheid Wall Micropillars

Wood's increasing role as a structural resource in sustainable materials selection demands accurate characterization of its mechanical behavior. Its performance arises from a hierarchical structure, where the dominant load-bearing component is the S2 layer of tracheid cell walls-a thick, fiber-reinforced composite of cellulose microfibrils embedded in hemicelluloses and lignin. Due to the small dimensions and anisotropic nature of the S2 layer, mechanical testing presents significant challenges, particularly in producing homogeneous stress and strain fields. In this study, we apply micropillar compression (MPC) combined with digital image correlation (DIC) to Norway spruce tracheids, enabling direct and model-free strain measurements at the cell wall scale. Micropillars were oriented at different microfibril angles (MFAs), confirming the expected dependence of stiffness and yield stress on ultrastructural alignment, with higher stiffness and yield stress at low MFAs. For these under compression fibril-aligned kink bands occurred, while shear related failure was observed at higher angles. A parameter study on the acceleration voltage of the Scanning Electron Microscope revealed that electron beam exposure significantly degrades pillar integrity, which could explain data scatter and mechanical underestimation in earlier MPC studies. By controlling imaging protocols and using DIC-based strain measurements, we report the highest direct measurements of wood cell wall stiffness to date-up to 42 GPa for MFA=0°-closer matching micromechanical model predictions compared to previous results. Findings are compared with Finite Element Method-based displacement corrections to establish a robust protocol for probing soft, anisotropic biological composites' mechanical behavior while clarifying longstanding inconsistencies in reported results of wood MPC measurements.

physics.bio-ph↗

arXiv2024

Fabrication and extreme micromechanics of additive metal microarchitectures

The mechanical performance of metallic metamaterials with 3-dimensional solid frames is typically a combination of the geometrical effect ("architecture") and the characteristic size effects of the base material ("microstructure"). In this study, for the first time, the temperature- and rate-dependent mechanical response of copper microlattices has been investigated. The microlattices were fabricated via a localized electrodeposition in liquid (LEL) process which enables high-precision additive manufacturing of metal at the micro-scale. The metal microlattices possess a unique microstructure with micron sized grains that are rich with randomly oriented growth twins and near-ideal nodal connectivity. Importantly, copper microlattices exhibited unique temperature (-150 and 25 degree C) and strain rate (0.001~100 s-1) dependent deformation behavior during in situ micromechanical testing. Systematic compression tests of fully dense copper micropillars, equivalent in diameter and length to the struts of the microlattice at comparable extreme loading conditions, allow us to investigate the intrinsic deformation mechanism of copper. Combined with the post-mortem microstructural analysis, substantial shifts in deformation mechanisms depending on the temperature and strain rate were revealed. On the one hand, at room temperature (25 degree C), dislocation slip based plastic deformation occurs and leads to a localized deformation of the micropillars. On the other hand, at cryogenic temperature (-150 degree C), mechanical twinning occurs and leads to relatively homogeneous deformation of the micropillars. Based on the intrinsic deformation mechanisms of copper, the temperature and strain rate dependent deformation behavior of microlattices could be explained.

cond-mat.mtrl-sci↗

arXiv2023

Enhanced mechanical properties and microstructural stability of ultrafine-grained biodegradable Zn-Li-Mn-Mg-Cu alloys produced by rapid solidification and high-pressure torsion

Zinc alloys have emerged as promising candidates for biodegradable materials due to their remarkable biocompatibility and favorable mechanical characteristics. The incorporation of alloying elements plays an essential role in advancing the tensile strength of Zn alloys. Nevertheless, achieving uniform dispersion of these elements poses challenges due to chemical segregation during solidification. In this study, rapid solidification followed by high-pressure torsion was successfully employed to fabricate Zn-Li-Mn-Mg-Cu alloys characterized by ultrafine-grained microstructures with evenly distributed nanometric intermetallic phases. A comprehensive examination, including phase composition, microstructural evolution, tensile properties and deformation mechanisms, was conducted. The impact of varying annealing temperatures on microstructural stability was systematically examined. The combined implementation of rapid solidification and high-pressure torsion yielded alloys with an average grain size below 360 nm, thereby demonstrating exceptional mechanical properties including yield stress (YS), ultimate tensile strength (UTS), and elongation to failure (Ef) equal to at least 325+-6 MPa, 350+-8 MPa and 40+-11 %, respectively. Heat treatment notably augmented the mechanical properties, resulting in a YS = 440+-11 MPa and UTS = 491+-6 MPa, while preserving plasticity (Ef = 23+-4 %) in the Zn-0.33Li-0.27Mn-0.14Mg-0.1Cu alloy. Nanoindentation strain rate jump tests identified thermally activated mechanisms and grain boundary sliding as dominant deformation mechanisms.

cond-mat.mtrl-sci↗

arXiv2022

Anomalous High Strain Rate Compressive Behavior of Additively Manufactured Copper Micropillars

Microscale dynamic testing is vital to the understanding of material behavior at application relevant strain rates. However, despite two decades of intense micromechanics research, the testing of microscale metals has been largely limited to quasi-static strain rates. Here we report the dynamic compression testing of pristine 3D printed copper micropillars at strain rates from $\sim0.001$ s$^{-1}$ to $\sim500$ s$^{-1}$. It was identified that microcrystalline copper micropillars deform in a single-shear like manner exhibiting a weak strain rate dependence at all strain rates. Ultrafine grained (UFG) copper micropillars, however, deform homogenously via barreling and show strong rate-dependence and small activation volumes at strain rates up to $\sim0.1$ s$^{-1}$, suggesting dislocation nucleation as the deformation mechanism. At higher strain rates, yield stress saturates remarkably, resulting in a decrease of strain rate sensitivity by two orders of magnitude and a four-fold increase in activation volume, implying a transition in deformation mechanism to collective dislocation nucleation.

cond-mat.mtrl-sci↗