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Jiawei Mi

Publications and source records attributed to Jiawei Mi.

5 recordsLinked to original sources

Revealing mesoscale bubble and particle dynamics in ultrasound-driven multiphase fluids by ultrafast synchrotron X-ray radiography and hybrid modelling

Multiphase fluid flows comprising of mesoscale solid particles, liquid droplets, or gas bubbles are common in both natural and man-made systems, but quantifying the energy transfer is challenging due to complex bubble-particle interactions. In this study, we used ultrafast synchrotron X-ray imaging to study the mesoscale dynamic interactions among ultrasonic cavitation bubbles and hydrophobic particles or clusters. Critical dynamic information and data were extracted from the vast amount of X-ray images and then fed into the hybrid analytical-numerical model for calculating the energy transfer from the oscillating bubble and the imploding bubble to the nearby hydrophobic particles. Using the Ni spherical microparticles as an example, at bubble oscillation approximately 16% (80-320 nJ) of the local energy was transferred to the particle. At bubble implosion, the transferred energy increased approximately 26% (0.135-1.09 uJ). Local energy transfer occurred on timescales of 1 us to 1 ms and length scales of 1 um to 1 mm. Within each ultrasound cycle, kinetic and potential energy underwent complex exchanges, with local energy exhibiting a stepwise decay at the end of each cycle. The transferred energy was mainly consumed for enabling highly efficient particle dispersion. This research provides quantitative insights into optimizing hydrophobic nanomaterial dispersion and has broader implications for interfacial energy transfer processes such as making suspensions, composite materials and exfoliated 2D materials.

physics.flu-dyn

Operando study of the evolution of peritectic structures in metal solidification by quasi-simultaneous synchrotron X-ray diffraction and tomography

Using quasi-simultaneous synchrotron X-ray diffraction and tomography techniques, we have studied in-situ and in real-time the nucleation and co-growth dynamics of the peritectic structures in an Al-Mn alloy during solidification. We collected ~30 TB 4D datasets which allow us to elucidate the phases' co-growth dynamics and their spatial, crystallographic and compositional relationship. The primary Al4Mn hexagonal prisms nucleate and grow with high kinetic anisotropy -70 times faster in the axial direction than the radial direction. In all cases, a ~5 um Mn-rich diffusion layer forms at the liquid-solid interface, creating a sharp local solute gradient that governs subsequent phase transformation. The peritectic Al6Mn phases nucleate epitaxially within this diffusion zone, initially forming a thin shell surrounding the Al4Mn with an orientation relationship of {10-10}HCP // {110}O, [0001]HCP // [001]O. Such ~5 um Mn-rich diffusion layers also cause solute depletion at the liquid side of the liquid-solid interface, limiting further epitaxial phase growth, but prompting phase re-nucleation and branching at crystal edges, resulting tetragonal prism structures that no longer follow the initial orientation relationship. The anisotropic diffusion also led to the formation of core defects at the centre of both phases. Furthermore, increasing cooling rate from 0.17 to 20 {\deg}C/s can disrupt the stability of the solute diffusion zone, effectively suppressing the formation of the core defects and forcing a transition from faceted to non-faceted morphologies. Our work establishes a new theoretical framework for how to tailor and control the peritectic structures in metallic alloys through solidification processes.

cond-mat.mtrl-sci

Ultrasound cavitation and exfoliation dynamics of 2D materials re-vealed in operando by X-ray free electron laser megahertz imaging

Ultrasonic liquid phase exfoliation is a promising method for the production of two-dimensional (2D) layered materials. A large number of studies have been made in investigating the underlying ultrasound exfoliation mechanisms. However, due to the experimental challenges for capturing the highly transient and dynamic phenomena in real-time at sub-microsecond time and micrometer length scales simultaneously, most theories reported to date still remain elusive. Here, using the ultra-short X-ray Free Electron Laser pulses (~25ps) with a unique pulse train structure, we applied MHz X-ray Microscopy and machine-learning technique to reveal unambiguously the full cycles of the ultrasound cavitation and graphite layer exfoliation dynamics with sub-microsecond and micrometer resolution. Cyclic fatigue shock wave impacts produced by ultrasound cloud implosion were identified as the dominant mechanism to deflect and exfoliate graphite layers mechanically. For the graphite flakes, exfoliation rate as high as ~5 angstroms per shock wave impact was observed. For the HOPG graphite, the highest exfoliation rate was ~0.15 angstroms per impact. These new findings are scientifically and technologically important for developing industrial upscaling strategies for ultrasonic exfoliation of 2D materials.

cond-mat.mtrl-sci

Non-destructive testing and evaluation of composite materials/structures: A state-of-the-art review

Composite materials/structures are advancing in product efficiency, cost-effectiveness and the development of superior specific properties. There are increasing demands in their applications to load-carrying structures in aerospace, wind turbines, transportation, and medical equipment, etc. Thus robust and reliable non-destructive testing (NDT) of composites is essential to reduce safety concerns and maintenance costs. There have been various NDT methods built upon different principles for quality assurance during the whole lifecycle of a composite product. This paper reviews the most established NDT techniques for detection and evaluation of defects/damage evolution in composites. These include acoustic emission, ultrasonic testing, infrared thermography, terahertz testing, shearography, digital image correlation, as well as X-ray and neutron imaging. For each NDT technique, we cover a brief historical background, principles, standard practices, equipment and facilities used for composite research. We also compare and discuss their benefits and limitations, and further summarise their capabilities and applications to composite structures. Each NDT technique has its own potential and rarely achieves a full-scale diagnosis of structural integrity. Future development of NDT techniques for composites will be directed towards intelligent and automated inspection systems with high accuracy and efficient data processing capabilities.

physics.app-ph

3D characterization of the primary Al3Sc phases in an Al-Sc alloy using Synchrotron X-ray tomography and electron microscopy

The three-dimensional structures of the primary Al3Sc particles in an Al-2Sc master alloy were studied by synchrotron X-ray microtomography, scanning and transmission electron microscopy. The Al3Sc phases were found to be a single cube and a cluster of cubes. The surface area, equivalent diameter of the Al3Sc cubes increased with the increasing of cube volume, but the specific surface area decreases. The primary Al3Sc cubes and Al-matrix have the same crystal orientation, indicating that the Al3Sc phases are the heterogeneous nucleation sites for Al. The experimental results show that α-Al2O3 are the possible nucleation sites for the Al3Sc cubes.

cond-mat.mtrl-sci