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Johannes A. Österreicher

Publications and source records attributed to Johannes A. Österreicher.

2 recordsLinked to original sources

DSC curve fingerprints directly encode mechanical properties of aluminum alloys

Differential scanning calorimetry (DSC) is a standard tool for studying precipitation and phase transformations in aluminum alloys, yet its relation to mechanical performance has so far remained mostly indirect. Here, we demonstrate that DSC curves themselves act as fingerprints that directly encode mechanical properties. Four representative 6xxx series alloys (Al-Mg-Si) were subjected to different natural and artificial aging regimens, followed by DSC heat-flow measurements and tensile testing. Machine learning models trained on the thermograms predicted yield strength, ultimate tensile strength, and uniform elongation in five-fold grouped cross-validation, with the best model (Lasso) achieving R^2 values of 0.93, 0.86, and 0.87 and mean absolute errors of 14.3 MPa, 11.1 MPa, and 1.5 percent, respectively. Leave-one-alloy-out evaluation with sparse calibration using anchor samples further demonstrated generalization across alloy chemistries. While direct prediction on unseen alloy data degraded performance substantially, inclusion of as few as one to two anchor conditions from the target alloy recovered predictive accuracy, approaching that of the standard cross-validation. Feature importance analysis revealed that the 230 to 270 C region, associated with precipitation of the primary hardening phase beta'', contributed most strongly to predictive accuracy, providing direct mechanistic validation of the model. These findings establish DSC as a diagnostic tool that can serve as a rapid proxy for mechanical property evaluation, enabling accelerated alloy screening, process optimization, and integration of thermal analysis into data-driven manufacturing.

cond-mat.mtrl-sci↗

Unlocking nanoscale microstructural detail in aluminium alloys through differential phase contrast segmentation in STEM

Differential phase contrast (DPC) imaging in scanning transmission electron microscopy (STEM) maps projected electric fields through the phase sensitivity of segmented low-angle detectors. Although typically applied to atomic-resolution imaging at low beam currents, STEM-DPC is here demonstrated as a rapid micro- and nanoscale image-segmentation tool for materials characterization in advanced aluminium alloys. Decomposition of false-colour DPC micrographs in hue-saturation-value space enables simultaneous identification and quantification of nanoclusters, GP zones, intermediate precipitate phases, dislocation cores, and associated strain fields within a single field of view. The method is demonstrated across multiple alloy systems, including clustering and strain-field mapping in a deformed AlMgZn(Cu) crossover alloy, precipitate identification in a paint-baked automotive sheet alloy, phase-variant segmentation in overaged AA7075-T7, and nanopore and nanoparticle detection in an anodic coating on AA2024-T3. Coupling DPC with neural-network segmentation further enables automated grain-boundary delineation and quantification in nanocrystalline aluminium thin films. Combined with STEM-EDX, DPC-based segmentation enables correlative microstructural analysis, establishing DPC as a rapid complement to techniques such as SPED and 4D-STEM.

cond-mat.mtrl-sci↗