arXiv subjects

M. Granata

Publications and source records attributed to M. Granata.

15 recordsLinked to original sources

arXiv2026

Experimental Realization of Optimized Ternary Mirror Coatings

We report on the first experimental realization of multi-material dielectric mirror coatings designed through a multi-objective optimization algorithm to simultaneously minimize thermal noise and optical losses. We validate this design strategy by fabricating and characterizing two distinct ternary systems: a SiNx -based proof-of-concept and a Ti:GeO2 -based system targeting lower optical losses. The performance of the SiN x coating shows remarkable agreement with predictions, demonstrating a noise amplitude spectral density reduction of 0.82 with respect to current reference coatings, and validating our design-to-fabrication pipeline. The Ti:GeO2 -based system achieves the crucial goal of sub-ppm absorption; its measured thermal noise, however, is higher than the theoretically predicted level of 0.71, extrapolated from single-layer material characterization. A dedicated tolerance analysis confirms that this discrepancy is not attributable to random thickness errors, emphasizing that further studies of the manufacturing process are needed to fully exploit this combination of materials. This work establishes a robust methodology for producing complex, high-performance optical coatings tailored for precision experiments.

physics.optics↗

arXiv2024

Development of ion-beam sputtered silicon nitride thin films for low-noise mirror coatings of gravitational-wave detectors

Brownian thermal noise of thin-film coatings is a fundamental limit for high-precision experiments based on optical resonators such as gravitational-wave interferometers. Here we present the results of a research activity aiming to develop lower-noise ion-beam sputtered silicon nitride thin films compliant with the very stringent requirements on optical loss of gravitational-wave interferometers. In order to test the hypothesis of a correlation between the synthesis conditions of the films and their elemental composition and optical and mechanical properties, we varied the voltage, current intensity and composition of the sputtering ion beam, and we performed a broad campaign of characterizations. While the refractive index was found to monotonically depend on the beam voltage and linearly vary with the N/Si ratio, the optical absorption appeared to be strongly sensitive to other factors, as yet unidentified. However, by systematically varying the deposition parameters, an optimal working point was found. Thus we show that the loss angle and extinction coefficient of our thin films can be as low as $(1.0 \pm 0.1) \times 10^{-4}$ rad at $\sim$2.8 kHz and $(6.4 \pm 0.2) \times 10^{-6}$ at 1064 nm, respectively, after thermal treatment at 900 $^{\circ}$C. To the best of our knowledge, such loss angle value is the lowest ever measured on this class of thin films. We then used our silicon nitride thin films to design and produce a multi-material mirror coating showing a thermal noise amplitude of $(10.3 \pm 0.2) \times 10^{-18}$ m Hz$^{-1/2}$ at 100 Hz, which is 25\% lower than in current mirror coatings of the Advanced LIGO and Advanced Virgo interferometers, and an optical absorption as low as $(1.6 \pm 0.5)$ parts per million at 1064 nm.

physics.ins-det↗

arXiv2023

Determination of compressive stress in thin films using micro-machined buckled membranes

In this work, optical profilometry and finite-element simulations are applied on buckled micro-machined membranes for the stress analysis of ion-beam-sputtered $\mathrm{Ta_{2}O_{5}}$ and $\mathrm{SiO_{2}}$ thin films. Layers with different thicknesses are grown on silicon substrates, then several membranes with different geometries are manufactured with standard micro-system technologies; due to a high level of the films' compressive stress, buckled membranes are obtained. Thermally-grown silica membranes are also produced, for comparison. The residual stress values are determined by comparing the measured and simulated deflections of the membranes. The average stress state of the $\mathrm{Ta_{2}O_{5}}$ thin films is found to be $-209$ MPa. The $\mathrm{SiO_{2}}$ thin films are in a higher compressive stress state whose average value is $-576$ MPa. The average stress in thermal $\mathrm{SiO_{2}}$ thin layers grown at 1130 $^{\circ}$C is found equal to $-321$ MPa, in good agreement with the literature.

physics.app-ph↗

arXiv2022

Characterization of ion-beam-sputtered AlF$_3$ thin films for gravitational-wave interferometers

Thermal noise in amorphous coatings is a limitation for a wide range of precision experiments such as gravitational-wave detectors (GWDs). Mirrors for GWDs are composed of multiple thin layers of dielectric materials deposited on a substrate: the stack is made of layers with a high refractive index interleaved with layers of a low refractive index. The goal is to obtain high reflectivity and low thermal noise. In this paper we report on the optical and mechanical properties of ion-beam-sputtered aluminium fluoride (AlF$_3$) thin films which have one of the lowest refractive index among the known coating materials and we discuss their application in current and future GWDs.

physics.ins-det↗

arXiv2022

Measurement and simulation of mechanical and optical properties of sputtered amorphous SiC coatings

In this work We report on the extensive characterization of amorphous silicon carbide (a-SiC) coatings prepared by physical deposition methods. We compare the results obtained on two different sputtering systems (a standard RF magnetron sputtering and a ion-beam assisted sputtering) to seize the impact of two different setups on the repeatably of the results. After a thorough characterization of structural, morphological, and compositional characteristics of the prepared samples, we focus on a detailed study of the optical and mechanical losses in those materials. Mechanical losses are further investigated from a microscopic point of view by comparing our experimental results with molecular dynamic simulations of the amorphous SiC structure: first we define a protocol to generate a numerical model of the amorphous film, capturing the main features of the real system; then we simulate its dynamical behaviour upon deformation in order to obtain its mechanical response. Our results are discussed within the perspective application of a-SiC as an optical material for high-precision optical experiments and in particular in gravitational wave interferometry.

physics.ins-det↗

arXiv2021

Optical and mechanical properties of ion-beam-sputtered MgF$_2$ thin films for gravitational-wave interferometers

Brownian thermal noise associated with highly reflective coatings is a fundamental limit for several precision experiments, including gravitational-wave detectors. Research is currently ongoing to find coatings with low thermal noise that also fulfill strict optical requirements such as low absorption and scatter. We report on the optical and mechanical properties of ion-beam-sputtered magnesium fluoride thin films, and we discuss the application of such coatings in current and future gravitational-wave detectors.

physics.ins-det↗

arXiv2021

Exploration of co-sputtered Ta$_2$O$_5$-ZrO$_2$ thin films for gravitational-wave detectors

We report on the development and extensive characterization of co-sputtered tantala-zirconia thin films, with the goal to decrease coating Brownian noise in present and future gravitational-wave detectors. We tested a variety of sputtering processes of different energies and deposition rates, and we considered the effect of different values of cation ratio $\eta =$ Zr/(Zr+Ta) and of post-deposition heat treatment temperature $T_a$ on the optical and mechanical properties of the films. Co-sputtered zirconia proved to be an efficient way to frustrate crystallization in tantala thin films, allowing for a substantial increase of the maximum annealing temperature and hence for a decrease of coating mechanical loss. The lowest average coating loss was observed for an ion-beam sputtered sample with $\eta = 0.485 \pm 0.004$ annealed at 800 $^{\circ}$C, yielding $\overline{\varphi} = 1.8 \times 10^{-4}$. All coating samples showed cracks after annealing. Although in principle our measurements are sensitive to such defects, we found no evidence that our results were affected. The issue could be solved, at least for ion-beam sputtered coatings, by decreasing heating and cooling rates down to 7 $^{\circ}$C/h. While we observed as little optical absorption as in the coatings of current gravitational-wave interferometers (0.5 parts per million), further development will be needed to decrease light scattering and avoid the formation of defects upon annealing.

physics.ins-det↗

arXiv2021

Optical and mechanical properties of ion-beam-sputtered Nb$_2$O$_5$ and TiO$_2$-Nb$_2$O$_5$ thin films for gravitational-wave interferometers

Brownian thermal noise associated with highly-reflective mirror coatings is a fundamental limit for several precision experiments, including gravitational-wave detectors. Recently, there has been a worldwide effort to find mirror coatings with improved thermal noise properties that also fulfill strict optical requirements such as low absorption and scatter. We report on the optical and mechanical properties of ion-beam-sputtered niobia and titania-niobia thin films, and we discuss application of such coatings in current and future gravitational-wave detectors. We also report an updated direct coating thermal noise measurement of the HR coatings used in Advanced LIGO and Advanced Virgo.

physics.ins-det↗

arXiv2014

Reconstruction of the gravitational wave signal $h(t)$ during the Virgo science runs and independent validation with a photon calibrator

The Virgo detector is a kilometer-scale interferometer for gravitational wave detection located near Pisa (Italy). About 13 months of data were accumulated during four science runs (VSR1, VSR2, VSR3 and VSR4) between May 2007 and September 2011, with increasing sensitivity. In this paper, the method used to reconstruct, in the range 10 Hz-10 kHz, the gravitational wave strain time series $h(t)$ from the detector signals is described. The standard consistency checks of the reconstruction are discussed and used to estimate the systematic uncertainties of the $h(t)$ signal as a function of frequency. Finally, an independent setup, the photon calibrator, is described and used to validate the reconstructed $h(t)$ signal and the associated uncertainties. The uncertainties of the $h(t)$ time series are estimated to be 8% in amplitude. The uncertainty of the phase of $h(t)$ is 50 mrad at 10 Hz with a frequency dependence following a delay of 8 $μ$s at high frequency. A bias lower than $4\,\mathrm{μs}$ and depending on the sky direction of the GW is also present.

gr-qc↗

arXiv2012

Scientific Potential of Einstein Telescope

Einstein gravitational-wave Telescope (ET) is a design study funded by the European Commission to explore the technological challenges of and scientific benefits from building a third generation gravitational wave detector. The three-year study, which concluded earlier this year, has formulated the conceptual design of an observatory that can support the implementation of new technology for the next two to three decades. The goal of this talk is to introduce the audience to the overall aims and objectives of the project and to enumerate ET's potential to influence our understanding of fundamental physics, astrophysics and cosmology.

gr-qc↗

arXiv2012

Scientific Objectives of Einstein Telescope

The advanced interferometer network will herald a new era in observational astronomy. There is a very strong science case to go beyond the advanced detector network and build detectors that operate in a frequency range from 1 Hz-10 kHz, with sensitivity a factor ten better in amplitude. Such detectors will be able to probe a range of topics in nuclear physics, astronomy, cosmology and fundamental physics, providing insights into many unsolved problems in these areas.

gr-qc↗

arXiv2011

Characterization of the Virgo Seismic Environment

The Virgo gravitational wave detector is an interferometer (ITF) with 3km arms located in Pisa, Italy. From July to October 2010, Virgo performed its third science run (VSR3) in coincidence with the LIGO detectors. Despite several techniques adopted to isolate the interferometer from the environment, seismic noise remains an important issue for Virgo. Vibrations produced by the detector infrastructure (such as air conditioning units, water chillers/heaters, pumps) are found to affect Virgo's sensitivity, with the main coupling mechanisms being through beam jitter and scattered light processes. The Advanced Virgo (AdV) design seeks to reduce ITF couplings to environmental noise by having most vibration-sensitive components suspended and in-vacuum, as well as muffle and relocate loud machines. During the months of June and July 2010, a Guralp-3TD seismometer was stationed at various locations around the Virgo site hosting major infrastructure machines. Seismic data were examined using spectral and coherence analysis with seismic probes close to the detector. The primary aim of this study was to identify noisy machines which seismically affect the ITF environment and thus require mitigation attention. Analyzed machines are located at various distances from the experimental halls, ranging from 10m to 100m. An attempt is made to measure the attenuation of emitted noise at the ITF and correlate it to the distance from the source and to seismic attenuation models in soil.

gr-qc↗

arXiv2011

Calibration and sensitivity of the Virgo detector during its second science run

The Virgo detector is a kilometer-length interferometer for gravitational wave detection located near Pisa (Italy). During its second science run (VSR2) in 2009, six months of data were accumulated with a sensitivity close to its design. In this paper, the methods used to determine the parameters for sensitivity estimation and gravitational wave reconstruction are described. The main quantities to be calibrated are the frequency response of the mirror actuation and the sensing of the output power. Focus is also put on their absolute timing. The monitoring of the calibration data as well as the parameter estimation with independent techniques are discussed to provide an estimation of the calibration uncertainties. Finally, the estimation of the Virgo sensitivity in the frequency-domain is described and typical sensitivities measured during VSR2 are shown.

gr-qc↗

arXiv2010

Sensitivity Studies for Third-Generation Gravitational Wave Observatories

Advanced gravitational wave detectors, currently under construction, are expected to directly observe gravitational wave signals of astrophysical origin. The Einstein Telescope, a third-generation gravitational wave detector, has been proposed in order to fully open up the emerging field of gravitational wave astronomy. In this article we describe sensitivity models for the Einstein Telescope and investigate potential limits imposed by fundamental noise sources. A special focus is set on evaluating the frequency band below 10Hz where a complex mixture of seismic, gravity gradient, suspension thermal and radiation pressure noise dominates. We develop the most accurate sensitivity model, referred to as ET-D, for a third-generation detector so far, including the most relevant fundamental noise contributions.

gr-qc↗

arXiv2010

Virgo calibration and reconstruction of the gravitational wave strain during VSR1

Virgo is a kilometer-length interferometer for gravitational waves detection located near Pisa. Its first science run, VSR1, occured from May to October 2007. The aims of the calibration are to measure the detector sensitivity and to reconstruct the time series of the gravitational wave strain h(t). The absolute length calibration is based on an original non-linear reconstruction of the differential arm length variations in free swinging Michelson configurations. It uses the laser wavelength as length standard. This method is used to calibrate the frequency dependent response of the Virgo mirror actuators and derive the detector in-loop response and sensitivity within ~5%. The principle of the strain reconstruction is highlighted and the h(t) systematic errors are estimated. A photon calibrator is used to check the sign of h(t). The reconstructed h(t) during VSR1 is valid from 10 Hz up to 10 kHz with systematic errors estimated to 6% in amplitude. The phase error is estimated to be 70 mrad below 1.9 kHz and 6 micro-seconds above.

gr-qc↗