arXiv subjects

M. Ziese

Publications and source records attributed to M. Ziese.

8 recordsLinked to original sources

arXiv2011

Evidence of defect-induced ferromagnetism in ZnFe$_{2}$O$_{4}$ thin films

X-ray absorption near-edge and grazing incidence X-ray fluorescence spectroscopy are employed to investigate the electronic structure of ZnFe$_{2}$O$_{4}$ thin films. The spectroscopy techniques are used to determine the non-equilibrium cation site occupancy as a function of depth and oxygen pressure during deposition and its effects on the magnetic properties. It is found that low deposition pressures below 10$^{-3}$ mbar cause iron superoccupation of tetrahedral sites without Zn$^{2+}$ inversion, resulting in an ordered magnetic phase with high room temperature magnetic moment.

cond-mat.mtrl-sci↗

arXiv2011

Are magnetite (Fe3O4) films on MgAl2O4 auxetic?

Magnetite (Fe3O4) films were fabricated on MgAl2O4 (001) single crystal substrates by pulsed laser deposition. In-plane and out-of-plane lattice constants were determined by X-ray diffraction. The apparent Poisson's ratio was determined as the negative ratio of the out-of-plane to in-plane strains. The results show that (i) the determination of Poisson's ratio by this method is only reliable for fully strained films and (ii) Poisson's ratio = 0.3 along the <100> direction is positive for this archetypal ferrite. Fe3O4 films grown on MgAl2O4 (001) are not auxetic.

cond-mat.mtrl-sci↗

arXiv2011

Magnetic Properties of Pr0.7Ca0.3MnO3/SrRuO3 Superlattices

High-quality Pr0.7Ca0.3MnO3/SrRuO3 superlattices were fabricated by pulsed laser deposition and were investigated by high-resolution transmission electron microscopy and SQUID magnetometry. Superlattices with orthorhombic and tetragonal SrRuO3 layers were investigated. The superlattices grew coherently; in the growth direction Pr0.7Ca0.3MnO3 layers were terminated by MnO2- and SrRuO3 layers by RuO2-planes. All superlattices showed antiferromagnetic interlayer coupling in low magnetic fields. The coupling strength was significantly higher for orthorhombic than for tetragonal symmetry of the SrRuO3 layers. The strong interlayer exchange coupling in the superlattice with orthorhombic SrRuO3 layers led to a magnetization reversal mechanism with a partially inverted hysteresis loop.

cond-mat.str-el↗

arXiv2011

Orthorhombic to tetragonal transition of SrRuO3 layers in Pr0.7Ca0.3MnO3/SrRuO3 superlattices

High-quality Pr0.7Ca0.3MnO3/SrRuO3 superlattices with ultrathin layers were fabricated by pulsed laser deposition on SrTiO3 substrates. The superlattices were studied by atomically resolved scanning transmission electron microscopy, high-resolution transmission electron microscopy, resistivity and magnetoresistance measurements. The superlattices grew coherently without growth defects. Viewed along the growth direction, SrRuO3 and Pr0.7Ca0.3MnO3 layers were terminated by RuO2 and MnO2, respectively, which imposes a unique structure to their interfaces. Superlattices with a constant thickness of the SrRuO3 layers, but varying thickness of the Pr0.7Ca0.3MnO3 layers showed a change of crystalline symmetry of the SrRuO3 layers. At a low Pr0.7Ca0.3MnO3 layer thickness of 1.5 nm transmission electron microscopy proved the SrRuO3 layers to be orthorhombic, whereas these were non-orthorhombic for a Pr0.7Ca0.3MnO3 layer thickness of 4.0 nm. Angular magnetoresistance measurements showed orthorhombic (with small monoclinic distortion) symmetry in the first case and tetragonal symmetry of the SrRuO3 layers in the second case. Mechanisms driving this orthorhombic to tetragonal transition are briefly discussed.

cond-mat.str-el↗

arXiv2009

Andreev reflection measurements in nanostructures with amorphous WC$_x$ superconducting contacts

Point-contact Andreev reflection measurements of Co/ and Cu/tungsten-carbide (WC$_x$) contacts are presented. Metallic thin films were patterned by e-beam-lithography and lift-off; tungsten carbide superconducting tips were grown directly on the pre-patterned samples by decomposition of a metallo-organic vapour (tungsten hexacarbonyl) under a focused Ga$^+$-ion beam (FIB). Current-voltage measurements as a function of temperature and magnetic field clearly showed the signatures of Andreev reflection. The experimental conductance-voltage curves were analyzed within the Blonder-Tinkham-Klapwijk theory. The results highlight the possibilities, advantages and disadvantages of using FIB-produced amorphous WC$_x$ tips for point-contact spectroscopy in metallic nanostructures.

cond-mat.supr-con↗

arXiv2007

Intrinsic Superconductivity at 25 K in Highly Oriented Pyrolytic Graphite

High resolution magnetoresistance data in highly oriented pyrolytic graphite thin samples manifest non-homogenous superconductivity with critical temperature $T_c \sim 25 $K. These data exhibit: i) hysteretic loops of resistance versus magnetic field similar to Josephson-coupled grains, ii) quantum Andreev's resonances and iii) absence of the Schubnikov-de Haas oscillations. The results indicate that graphite is a system with non-percolative superconducting domains immersed in a semiconducting-like matrix. As possible origin of the superconductivity in graphite we discuss interior-gap superconductivity when two very different electronic masses are present.

cond-mat.supr-con↗

arXiv2006

Direct Correlation between 1/f-magneto-noise and magnetoresistance in La0.7Sr0.3MnO3 and (La0.5Pr0.2)Ba0.3MnO3 manganites

Temperature- and magnetic field-dependent electrical noise and electrical resistivity measurements were carried out on epitaxial thin films of a large bandwidth La0.7Sr0.3MnO3 and a disordered intermediate bandwidth (La0.5Pr0.2)Ba0.3MnO3 manganite system. The power spectraldensity was dominated by 1/f-noise. This 1/f-noise was observed to follow the overall temperature dependence of the resistivity. Moreover, in these compounds the magneto-noise effect was found to be of nearly the same magnitude as the magnetoresistance. This direct correlation between magneto-noise and magnetoresistance suggests that the enhanced 1/f-noise has its origin in intrinsic charge-carrier density fluctuations.

cond-mat.str-el↗

arXiv2004

Searching for a magnetic proximity effect in magnetite-carbon structures

In order to study a possible magnetic proximity effect in magnetite-carbon structures, we have performed magnetization measurements of graphite-magnetite composites with different mass ratios as well as the measurement of the magnetoresistance of one of them and of the magnetization of a magnetite-carbon bilayer. The overall results do not indicate the induction of bulk ferromagnetism in graphite and disordered carbon structures through their contact with magnetite.

cond-mat.mtrl-sci↗