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Martin de Wit

Publications and source records attributed to Martin de Wit.

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System performance of a cryogenic test-bed for the time-division multiplexing readout for NewAthena X-IFU

The X-ray Integral Field Unit (X-IFU) is an instrument of ESA's future NewAthena space observatory, with the goal to provide high-energy resolution ($<$ 4 eV at X-ray energies up to 7 keV) and high-spatial resolution (9") spectroscopic imaging over the X-ray energy range from 200 eV to 12 keV, by means of an array of about 1500 transition-edge sensors (TES) read out via SQUID time-division multiplexing (TDM). A TDM-based laboratory test-bed has been assembled at SRON, hosting an array of $75\times 75\ \upmu$m$^2$ TESs that are read out via 2-column $\times$ 32-row TDM. A system component that is critical to high-performance operation is the wiring harness that connects the room-temperature electronics to the cryogenic readout componentry. We report here on our characterization of such a test-bed, whose harness has a length close to what envisioned for X-IFU, which allowed to achieve a co-added energy resolution at a level of 2.7~eV FWHM at 6~keV via 32-row readout. In addition, we provide an outlook on the integration of TDM readout into the X-IFU Focal-Plane Assembly Development Model.

astro-ph.IM

Demonstration of Weak-Link Physics in the Dynamical Response of Transition-Edge Sensors

We theoretically predict and experimentally observe the onset of weak-link physics in the dynamical response of transition edge sensors (TES). We develop a theoretical framework based on a Fokker-Planck description that incorporates both the TES electrical response, stemming from Josephson phenomena, and the electrothermal effects due to coupling to a thermal bath. Our measurements of a varying dynamic resistance are in excellent agreement with our theory, thereby establishing weak-link phenomena as the main mechanism underlying the operation of TES. Furthermore, our description enables the calculation of power spectral densities, paving the way for a more thorough investigation of the unexplained "excess noise" in long diffusive junctions and TES reported in recent experiments.

cond-mat.mes-hall

Increased muon field at surface and substrate interface of palladium thin films

We performed depth-dependent low-energy muon spin spectroscopy ($μ$SR) studies on three palladium 100 nm thin films, both undoped and doped with 170 ppm of iron. Muons implanted in the surface and substrate interface region probe an increased local magnetic field compared to the inner part of the sample. The field increase extends over a few nanometers, it is temperature-independent (in the range of 3.7 - 100 K), stronger for the iron-doped samples and accompanied by an increase in local field inhomogeneity. We consider various potential origins for this magnetic surface state, such as adsorbents and supressed d-states. Our conclusion is that orbital moments induced at the surface / interface by localized spins and charges are the most likely explanation, potentially accompanied by magnetic moments due to crystal irregularities.

cond-mat.mes-hall

Frequency domain multiplexing readout for large arrays of transition-edge sensors

We report our most recent progress and demonstration of a frequency domain multiplexing (FDM) readout technology for transition-edge sensor (TES) arrays, both of which we have been developing, in the framework of the X-IFU instrument on board the future Athena X-ray telescope. Using Ti/Au TES micro-calorimeters, high-Q LC filters and analog/digital electronics developed at SRON and low-noise two-stage SQUID amplifiers from VTT Finland, we demonstrated feasibility of our FDM readout technology, with the simultaneous readout of 37 pixels with an energy resolution at of 2.23 eV at an energy of 6 keV. We finally outline our plans for further scaling up and improving our technology.

astro-ph.IM

Performance of the SRON Ti/Au Transition Edge Sensor X-ray Calorimeters

In the early 2030s, ESAs new X-ray observatory, Athena, is scheduled to be launched. It will carry two main instruments, one of which is the X-ray Integral Field Unit (X-IFU), an X-ray imaging spectrometer, which will consist of an array of several thousand transition-edge sensors (TESs) with a proposed energy resolution of 2.5 eV for photon energies up to 7 keV. At SRON we develop the backup TES array based on Ti/Au bilayers with a transition temperature just below 100 mK. In this contribution we will give a broad overview of the properties and capabilities of these state-of-the-art detectors. Over the years we have fabricated and studied a large number of detectors with various geometries, providing us with a good understanding of how to precisely control the properties of our detectors. We are able to accurately vary the most important detector properties, such as the normal resistance, thermal conductance and critical temperature. This allows us to finely tune our detectors to meet the demands of various applications. The detectors have demonstrated excellent energy resolutions of below 1.8 eV for 5.9 keV X-rays. By tuning the properties of the devices, they can be optimally matched to various read-out schemes using both AC and DC biasing. The next step is to increase the size of our TES arrays from our current kilo-pixel arrays towards the full-sized array for X-IFU.

astro-ph.IM

Susceptibility study of TES micro-calorimeters for X-ray spectroscopy under FDM readout

We present a characterization of the sensitivity of TES X-ray micro-calorimeters to environmental conditions under frequency-domain multiplexing (FDM) readout. In the FDM scheme, each TES in a readout chain is in series with a LC band-pass filter and AC biased with an independent carrier at MHz range. Using TES arrays, cold readout circuitry and warm electronics fabricated at SRON and SQUIDs produced at VTT Finland, we characterize the sensitivity of the detectors to bias voltage, bath temperature and magnetic field. We compare our results with the requirements for the Athena X-IFU instrument, showing the compliance of the measured sensitivities. We find in particular that FDM is intrinsically insensitive to the magnetic field because of TES design and AC readout.

astro-ph.IM

Mitigation of the Magnetic Field Susceptibility of Transition Edge Sensors using a Superconducting Groundplane

Transition edge sensor (TES) microcalorimeters and bolometers are used for a variety of applications. The sensors are based on the steep temperature-dependent resistance of the normal-to-superconducting transition, and are thus intrinsically sensitive to magnetic fields. Conventionally the detectors are shielded from stray magnetic fields using external magnetic shields. However, in particular for applications with strict limits on the available space and mass of an instrument, external magnetic shields might not be enough to obtain the required shielding factors or field homogeneity. Additionally, these shields are only effective for magnetic fields generated external to the TES array, and are ineffective to mitigate the impact of internally generated magnetic fields. Here we present an alternative shielding method based on a superconducting groundplane deposited directly on the backside of the silicon nitride membrane on which the TESs are located. We demonstrate that this local shielding for external magnetic fields has a shielding factor of at the least ~ 75, and is also effective at reducing internal self-induced magnetic fields, as demonstrated by measurements and simulation of the eddy current losses in our AC biased detectors. Measurements of 5.9 keV X-ray photons show that our shielded detectors have a high resilience to external magnetic fields, showing no degradation of the energy resolution or shifts of the energy scale calibration for fields of several microTesla, values higher than expected in typical real-world applications.

astro-ph.IM

Thermal crosstalk of X-ray transition-edge sensor micro-calorimeters under frequency domain multiplexing readout

We have measured and characterized the thermal crosstalk in two different arrays of transition-edge sensor (TES) X-ray micro-calorimeters with frequency-domain multiplexing (FDM) readout. The TES arrays are fabricated at SRON and are a 8$\times$8 and a 32$\times$32 "kilo-pixel" uniform array. The amount of crosstalk is evaluated as the ratio between the averaged crosstalk signal and the X-ray pulse amplitudes. The crosstalk ratios (CR) for our detectors are compliant with the requirements for future X-ray space missions, such as Athena X-IFU (CR$< 10^{-3}$ for first-neighbour pixels): we measured a nearest-neighbour thermal crosstalk ratio at a level of $10^{-4}$, with a highest crosstalk ratio of $4\times 10^{-4}$ for the kilo-pixel array (worst case, center of array) and $1\times 10^{-4}$ for the 8$\times$8 array, with a margin of improvement achievable by optimizing the Cu metallization and the width of the Si supporting structures (muntins) in the backside of the TES array chip. Based on the measured crosstalk ratios, we have estimated the impact on the spectral resolution by means of noise equivalent power (NEP) considerations and a Monte Carlo simulation, finding an average degradation in quadrature of less than 40~meV, compliant with the < 0.2~eV requirement for Athena X-IFU.

astro-ph.IM

Single pixel performance of a 32$\times$32 Ti/Au TES array with broadband X-ray spectra

We are developing a kilo-pixels Ti/Au TES array as a backup option for Athena X-IFU. Here we report on single-pixel performance of a 32$\times$32 array operated in a Frequency Division Multiplexing (FDM) readout system, with bias frequencies in the range 1-5 MHz. We have tested the pixels response at several photon energies, by means of a $^{55}$Fe radioactive source (emitting Mn-K$α$ at 5.9 keV) and a Modulated X-ray Source (MXS, providing Cr-K$α$ at 5.4 keV and Cu-K$α$ at 8.0 keV). First, we report the procedure used to perform the detector energy scale calibration, usually achieving a calibration accuracy better than $\sim$ 0.5 eV in the 5.4 - 8.9 keV energy range. Then, we present the measured energy resolution at the different energies (best single pixel performance: $Δ$E$_{FWHM}$ = 2.40 $\pm$ 0.09 eV @ 5.4 keV; 2.53 $\pm$ 0.10 eV @ 5.9 keV; 2.78 $\pm$ 0.16 eV @ 8.0 keV), investigating also the performance dependency from the pixel bias frequency and the count rate. Thanks to long background measurements ($\sim$ 1 day), we finally detected also the Al-K$α$ line at 1.5 keV, generated by fluorescence inside the experimental setup. We analyzed this line to obtain a first assessment of the single-pixel performance also at low energy ($Δ$E$_{FWHM}$ = 1.91 eV $\pm$ 0.21 eV @ 1.5 keV), and to evaluate the linearity of the detector response in a large energy band (1.5 - 8.9 keV).

astro-ph.IM

Flux compensation for SQUID-detected Magnetic Resonance Force Microscopy

One of the major challenges in performing SQUID-detected Magnetic Resonance Force Microscopy (MRFM) at milliKelvin temperatures is the crosstalk between the radiofrequency (RF) pulses used for the spin manipulation and the SQUID-based detection mechanism. Here we present an approach based on balancing the flux crosstalk using an on-chip feedback coil coupled to the SQUID. This approach does not require any additional components near the location of the sample, and can therefore be applied to any SQUID-based detection scheme to cancel predictable RF interference. We demonstrate the effectiveness of our approach by showing that we can almost completely negate flux crosstalk with an amplitude of up to several $Φ_0$. This technical achievement allows for complicated magnetic resonance protocols to be performed at temperatures below 50 mK.

physics.app-ph

Vibration isolation with high thermal conductance for a cryogen-free dilution refrigerator

We present the design and implementation of a mechanical low-pass filter vibration isolation used to reduce the vibrational noise in a cryogen-free dilution refrigerator operated at 10 mK, intended for scanning probe techniques. We discuss the design guidelines necessary to meet the competing requirements of having a low mechanical stiffness in combination with a high thermal conductance. We demonstrate the effectiveness of our approach by measuring the vibrational noise levels of an ultrasoft mechanical resonator positioned above a SQUID. Starting from a cryostat base temperature of 8 mK, the vibration isolation can be cooled to 10.5 mK, with a cooling power of 113 $μ$W at 100 mK. We use the low vibrations and low temperature to demonstrate an effective cantilever temperature of less than 20 mK. This results in a force sensitivity of less than 500 zN/$\sqrt{\mathrm{Hz}}$, and an integrated frequency noise as low as 0.4 mHz in a 1 Hz measurement bandwidth.

physics.app-ph

Feasibility of imaging using Boltzmann polarization in nuclear Magnetic Resonance Force Microscopy

We report on Magnetic Resonance Force Microscopy measurements of the Boltzmann polarization of the nuclear spins in copper by detecting the frequency shift of a soft cantilever. We use the time-dependent solution of the Bloch equations to derive a concise equation describing the effect of rf magnetic fields on both on- and off-resonant spins in high magnetic field gradients. We then apply this theory to saturation experiments performed on a 100 nm thick layer of copper, where we use the higher modes of the cantilever as source of the rf field. We demonstrate a detection volume sensitivity of only (40 nm)$^3$, corresponding to about 1.6$\cdot 10^4$ polarized copper nuclear spins. We propose an experiment on protons where, with the appropriate technical improvements, frequency-shift based magnetic resonance imaging with a resolution better than (10 nm)$^3$ could be possible. Achieving this resolution would make imaging based on the Boltzmann polarization competitive with the more traditional stochastic spin-fluctuation based imaging, with the possibility to work at milliKelvin temperatures.

cond-mat.mes-hall

Density and $T_1$ of surface and bulk spins in diamond in high magnetic field gradients

We report on surface and bulk spin density measurements of diamond, using ultra-sensitive magnetic force microscopy with magnetic field gradients up to 0.5 T/$μ$m. At temperatures between 25 and 800 mK, we measure the shifts in the resonance frequency and quality factor of a cantilever with a micromagnet attached to it. A recently developed theoretical analysis allows us to extract a surface spin density of 0.072 spins/nm$^2$ and a bulk spin density of 0.4 ppm from this data. In addition, we find an increase of the $T_1$ time of the surface spins in high magnetic field gradients due to the suppression of spin diffusion. Our technique is applicable to a variety of samples other than diamond, and could be of interest for several research fields where surface, interface or impurity bulk spin densities are an important factor.

cond-mat.mes-hall