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O. Bourgeois

Publications and source records attributed to O. Bourgeois.

At least 19 recordsLinked to original sources

Voltage Noise Thermometry in Integrated Circuits at Millikelvin Temperatures

This paper demonstrates the use of voltage noise thermometry, with a cross-correlation technique, as a dissipation-free method of thermometry inside a CMOS integrated circuit (IC). We show that this technique exhibits broad agreement with the refrigerator temperature range from 300 mK to 8 K. Furthermore, it shows substantial agreement with both an independent in-IC thermometry technique and a simple thermal model as a function of power dissipation inside the IC. As the device under test (DUT) is a resistor, it is feasible to extend this technique by placing many resistors in an IC to monitor the local temperatures, without increasing IC design complexity. This could lead to better understanding of the thermal profile of ICs at cryogenic temperatures. This has its greatest potential application in quantum computing, where the temperature at the cold classical-quantum boundary must be carefully controlled to maintain qubit performance.

physics.app-ph

Experimental set-up for thermal measurements at the nanoscale using an SThM probe with niobium nitride thermometer

Scanning Thermal Microscopy (SThM) has become an important measurement tool for characterizing the thermal properties of materials at the nanometer scale. This technique requires a SThM probe that combines an Atomic Force Microscopy (AFM) probe and a very sensitive resistive thermometry; the thermometer being located at the apex of the probe tip allows the mapping of temperature or thermal properties of nanostructured materials with very high spatial resolution. The high interest of the SThM technique in the field of thermal nanoscience currently suffers from a low temperature sensitivity despite its high spatial resolution. To address this challenge, we developed a high vacuum-based AFM system hosting a highly sensitive niobium nitride (NbN) SThM probe to demonstrate its unique performance. As a proof of concept, we utilized this custom-built system to carry out thermal measurements using the 3$\omega$ method. By measuring the $V_{3\omega}$ voltage on the NbN resistive thermometer in vacuum conditions we were able to determine the SThM probe's thermal conductance and thermal time constant. The performance of the probe is demonstrated by doing thermal measurements in-contact with a sapphire sample.

cond-mat.mes-hall

On-chip thermometry for microwave optomechanics implemented in a nuclear demagnetization cryostat

We report on microwave optomechanics measurements performed on a nuclear adiabatic demagnetization cryostat, whose temperature is determined by accurate thermometry from below 500$~μ$K to about 1$~$Kelvin. We describe a method for accessing the on-chip temperature, building on the blue-detuned parametric instability and a standard microwave setup. The capabilities and sensitivity of both the experimental arrangement and the developed technique are demonstrated with a very weakly coupled silicon-nitride doubly-clamped beam mode of about 4$~$MHz and a niobium on-chip cavity resonating around 6$~$GHz. We report on an unstable intrinsic driving force in the coupled microwave-mechanical system acting on the mechanics that appears below typically 100$~$mK. The origin of this phenomenon remains unknown, and deserves theoretical input. It prevents us from performing reliable experiments below typically 10-30$~$mK; however no evidence of thermal decoupling is observed, and we propose that the same features should be present in all devices sharing the microwave technology, at different levels of strengths. We further demonstrate empirically how most of the unstable feature can be annihilated, and speculate how the mechanism could be linked to atomic-scale two level systems. The described microwave/microkelvin facility is part of the EMP platform, and shall be used for further experiments within and below the millikelvin range.

cond-mat.mes-hall

A macroscopic object passively cooled into its quantum ground state of motion: beyond single-mode cooling

The building blocks of Nature, namely atoms and elementary particles, are described by quantum mechanics. This fundamental theory is the ground on which physicists have built their major mathematical models [1]. Today, the unique features of quantum objects have led to the advent of promising quantum technologies [2, 3]. However, the macroscopic world is manifestly classical, and the nature of the quantum-to-classical crossover remains one of the most challenging open question of Science to date. In this respect, moving objects play a specific role [4, 5]. Pioneering experiments over the last few years have begun exploring quantum behaviour of micron-sized mechanical systems,either by passively cooling single GHz modes, or by adapting laser cooling techniques developed in atomic physics to cool specific modes far below the temperature of their surroundings [6-11]. Here instead we describe a very different approach, passive cooling of a micromechanical system down to 500 microK, reducing the average number of quanta in the fundamental vibrational mode at 15 MHz to just 0.3 (with even lower values expected for higher harmonics); the challenge being to be still able to detect the motion without disturbing the system noticeably. With such an approach higher harmonics and the surrounding environment are also cooled, leading to potentially much longer mechanical coherence times, and enabling experiments questioning mechanical wave-function collapse [12], potentially from the gravitational background [13, 14], and quantum thermodynamics [15]. Beyond the average behaviour, here we also report on the fluctuations of the fundamental vibrational mode of the device in-equilibrium with the cryostat. These reveal a surprisingly complex interplay with the local environment and allow characteristics of two distinct thermodynamic baths to be probed.

quant-ph

Specific Heat Signature of the Berezinskii-Kosterlitz-Thouless Transition in Ultrathin Superconducting Films

The Berezinskii-Kosterlitz-Thouless (BKT) transition is expected to have a clear signature on the specific heat. The singularity at the transition temperature $T_{BKT}$ is predicted to be immeasurable, and a broad non-universal peak is expected at $T>T_{BKT}$. Up to date this has not been observed in two-dimensional superconductors. We use a unique highly sensitive technique to measure the specific heat of ultrathin Pb films. We find that thick films exhibit a specific heat jump at $T_C$ that is consistent with BCS theory. As the film thickness is reduced below the superconducting coherence length and the systems enters the 2D limit the specific heat reveals BKT-like behavior. We discuss these observations in the framework of the continuous BCS-BKT crossover as a function of film thickness.

cond-mat.supr-con

Surface-induced near-field scaling in the Knudsen layer of a rarefied gas

We report on experiments performed within the Knudsen boundary layer of a low-pressure gas. The non-invasive probe we use is a suspended nano-electro-mechanical string (NEMS), which interacts with $^4$He gas at cryogenic temperatures. When the pressure $P$ is decreased, a reduction of the damping force below molecular friction $\propto P$ had been first reported in Phys. Rev. Lett. Vol 113, 136101 (2014) and never reproduced since. We demonstrate that this effect is independent of geometry, but dependent on temperature. Within the framework of kinetic theory, this reduction is interpreted as a rarefaction phenomenon, carried through the boundary layer by a deviation from the usual Maxwell-Boltzmann equilibrium distribution induced by surface scattering. Adsorbed atoms are shown to play a key role in the process, which explains why room temperature data fail to reproduce it.

cond-mat.mes-hall

Slippage and boundary layer probed in an almost-ideal gas by a nano-mechanical oscillator

We have measured the interaction between $^4$He gas at 4.2$~$K and a high-quality nano-electro-mechanical string device for its first 3 symmetric modes (resonating at 2.2$~$MHz, 6.7$~$MHz and 11$~$MHz with quality factor $Q > 0.1$ million) over almost 6 orders of magnitude in pressure. This fluid can be viewed as the best experimental implementation of an almost-ideal monoatomic and inert gas which properties are tabulated. The experiment ranges from high pressure where the flow is of laminar Stokes-type presenting slippage, down to very low pressures where the flow is molecular. In the molecular regime, when the mean-free-path is of the order of the distance between the suspended nano-mechanical probe and the bottom of the trench we resolve for the first time the signature of the boundary (Knudsen) layer onto the measured dissipation. Our results are discussed in the framework of the most recent theories investigating boundary effects in fluids (both analytic approaches and Monte-Carlo DSMC simulations).

cond-mat.mes-hall

Evidence for the role of normal-state electrons in nanoelectromechanical damping mechanisms at very low temperatures

We report on experiments performed at low temperatures on aluminum covered silicon nanoelectromechanical resonators. The substantial difference observed between the mechanical dissipation in the normal and superconducting states measured within the same device unambiguously demonstrates the importance of normal-state electrons in the damping mechanism. The dissipative component becomes vanishingly small at very low temperatures in the superconducting state, leading to exceptional values for the quality factor of such small silicon structures. A critical discussion is given within the framework of the standard tunneling model.

cond-mat.mes-hall

In-situ comprehensive calibration of a tri-port nano-electro-mechanical device

We report on experiments performed in vacuum and at cryogenic temperatures on a tri-port nano-electro-mechanical (NEMS) device. One port is a very non-linear capacitive actuation, while the two others implement the magnetomotive scheme with a linear input force port and a (quasi-linear) output velocity port. We present an experimental method enabling a full characterization of the nanomechanical device harmonic response: the non-linear capacitance function $C(x)$ is derived, and the normal parameters $k$ and $m$ (spring constant and mass) of the mode under study are measured through a careful definition of the motion (in meters) and of the applied forces (in Newtons). These results are obtained with a series of purely electric measurements performed without disconnecting/reconnecting the device, and rely only on known DC properties of the circuit, making use of a thermometric property of the oscillator itself: we use the Young modulus of the coating metal as a thermometer, and the resistivity for Joule heating. The setup requires only three connecting lines without any particular matching, enabling the preservation of a high impedance NEMS environment even at MHz frequencies. The experimental data are fit to a detailed electrical and thermal model of the NEMS device, demonstrating a complete understanding of its dynamics. These methods are quite general and can be adapted (as a whole, or in parts) to a large variety of elecromechanical devices.

cond-mat.mes-hall

Modal "self-coupling" as a sensitive probe for nanomechanical detection

We present a high-sensitivity measurement technique for mechanical nanoresonators. Due to intrinsic nonlinear effects, different flexural modes of a nanobeam can be coupled while driving each of them on resonance. This mode-coupling scheme is dispersive and one mode resonance shifts with respect to the motional amplitude of the other. The same idea can be implemented on a {\it single} mode, exciting it with two slightly detuned signals. This two-tone scheme is used here to measure the resonance lineshape of one mode through a frequency shift in the response of the device. The method acts as an amplitude-to-frequency transduction which ultimately suffers only from phase noise of the local oscillator used and of the nanomechanical device itself. We also present a theory which reproduces the data without free parameters.

cond-mat.mes-hall

Nonlinear parametric amplification in a tri-port nanoelectromechanical device

We report on measurements performed at low temperatures on a nanoelectromechanical system (NEMS) under (capacitive) parametric pumping. The excitations and detection schemes are purely electrical, and enable in the present experiment the straightforward measurement of forces down to about a femtonewton, for displacements of an Angström, using standard room temperature electronics. We demonstrate that a small (linear) force applied on the device can be amplified up to more than a 100 times, while the system is {\it truly moving}. We explore the dynamics up to about 50$~$nm deflections for cantilevers about 200$~$nm thick by 3$~$$μ$m long oscillating at a frequency of 7$~$MHz. We present a generic modeling of nonlinear parametric amplification, and give analytic theoretical solutions enabling the fit of experimental results. We finally discuss the practical limits of the technique, with a particular application: the measurement of {\it anelastic damping} in the metallic coating of the device with an exceptional resolution of about 0.5$~$\%.

cond-mat.mes-hall

Highly sensitive thermal conductivity measurements of suspended membranes (SiN and diamond) using a 3w-Volklein method

A suspended system for measuring the thermal properties of membranes is presented. The sensitive thermal measurement is based on the 3$ω$ dynamic method coupled to a V$\ddot{o}$lklein geometry. The device obtained using micro-machining processes allows the measurement of the in-plane thermal conductivity of a membrane with a sensitivity of less than 10nW/K (+/-$5x10^{-3}$Wm$^{-1}K^{-1}$ at room temperature) and a very high resolution ($ΔK/K =10^{-3}$). A transducer (heater/thermometer) centered on the membrane is used to create an oscillation of the heat flux and to measure the temperature oscillation at the third harmonic using a Wheatstone bridge set-up. Power as low as 0.1nanoWatt has been measured at room temperature. The method has been applied to measure thermal properties of low stress silicon nitride and polycrystalline diamond membranes with thickness ranging from 100 nm to 400 nm. The thermal conductivity measured on the polycrystalline diamond membrane support a significant grain size effect on the thermal transport.

cond-mat.mes-hall

Audio mixing in a tri-port nano-electro-mechanical device

We report on experiments performed on a cantilever-based tri-port nano-electro-mechanical (NEMS) device. Two ports are used for actuation and detection through the magnetomotive scheme, while the third port is a capacitively coupled gate electrode. By applying a low frequency voltage signal on the gate, we demonstrate mixing in the mechanical response of the device, even for {\it low magnetomotive drives, without resorting to conduction measurements through the NEMS}. The technique can thus be used in particular in the linear regime, as an alternative to nonlinear mixing, for normal conducting devices. An analytic theory is presented reproducing the data without free parameters

cond-mat.mes-hall

Phase-Dependent Electronic Specific Heat in Mesoscopic Josephson Junctions

We study the influence of superconducting correlations on the electronic specific heat in a diffusive superconductor-normal metal-superconductor Josephson junction. We present a description of this system in the framework of the diffusive-limit Green's function theory, taking into account finite temperatures, phase difference as well as junction parameters. We find that proximity effect may lead to a substantial deviation of the specific heat as compared to that in the normal state, and that it can be largely tuned in magnitude by changing the phase difference between the superconductors. A measurement setup to confirm these predictions is also suggested.

cond-mat.mes-hall

Non-equilibrium heat capacity of polytetrafluoroethylene at room temperature

Polytetrafluoroethylene can be considered as a model for calorimetric studies of complex systems with thermodynamics transitions at ambient temperature. This polymer exhibits two phase transitions of different nature at 292 K and 303 K. We show that sensitive ac-calorimetry measurements allow us to study the thermodynamic behaviour of polytetrafluoroethylene when it is brought out of thermodynamic equilibrium. Thanks to the thermal modelisation of our calorimetric device, the frequency dependent complex heat capacity of this polymer is extracted. The temperature and frequency variations of the real and imaginary parts of the complex heat capacity are obtained when polytetrafluoroethylene undergoes its first-order structural phase transition at 292 K.

cond-mat.soft

Specific heat measurement of mesoscopic loops

We report highly sensitive specific heat measurement on mesoscopic superconducting loops at low temperature. These mesoscopic systems exhibit thermal properties significantly different from that of the bulk materials. The measurement is performed on a silicon membrane sensor where 450 000 superconducting aluminium loops are deposited through electron beam lithography under an applied magnetic field. Each entry of a vortex is associated to a jump in the specific heat of few thousands of Boltzmann constant kB indicating the existence of phase transitions. The periodicity of this sequential phase transitions is a nontrivial behaviour and varies strongly as the temperature is decreased. The successive phase transitions are well described by the Ginzburg-Landau theory of superconductivity. The presence of metastable states is responsible for the n-0 (n=1, 2, 3...) periodicity of the discontinuities of the measured specific heat.

cond-mat.mes-hall

Attojoule calorimetry of mesoscopic superconducting loops

We report the first experimental evidence of nontrivial thermal behavior of the simplest mesoscopic system - a superconducting loop. By measuring the specific heat C of an array of 450,000 noninteracting aluminum loops with very high accuracy of ~20 fJ/K, we show that the loops go through a periodic sequence of phase transitions (with period of an integer number of magnetic flux quanta) as the magnetic flux threading each loop is increased. The transitions are well described by the Ginzburg-Landau theory and are accompanied by discontinuities of C of only several thousands of Boltzmann constants k_B.

cond-mat.mes-hall

Proximity effect in ultrathin Pb/Ag multilayers within the Cooper limit

We report on transport and tunneling measurements performed on ultra-thin Pb/Ag (strong coupled superconductor/normal metal) multilayers evaporated by quench condensation. The critical temperature and energy gap of the heterostructures oscillate with addition of each layer, demonstrating the validity of the Cooper limit model in the case of multilayers. We observe excellent agreement with a simple theory for samples with layer thickness larger than 30Å. Samples with single layers thinner than 30Ådeviate from the Cooper limit theory. We suggest that this is due to the "inverse proximity effect" where the normal metal electrons improve screening in the superconducting ultrathin layer and thus enhance the critical temperature.

cond-mat.supr-con