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Raoul Fix

Publications and source records attributed to Raoul Fix.

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A temperature dependent framework to predict and control physical pellet quality in biomass extrusion

Pellet manufacturing of biomass (food, feed, bioenergy) presses powders or particles into dense pellets with improved nutritional, calorific, and handling properties. This process upgrades industrial co-products from agriculture, forestry, and bioenergy into higher-value products. However, processing particulate streams raises the scientific question: Under which conditions do loose particles bind to form rigid, durable pellets? This work answers this question for biomass extrusion. Systematic experiments reveal how steam conditioning temperature, production rate, and die geometry interact to determine pellet quality. We propose an overarching framework introducing the stickiness temperature ($T^*$), marking the onset of enthalpic reactions required for particle agglomeration. $T^*$ serves as the boundary for inter-particle bond formation and is reached through a combination of steam conditioning and friction, both controllable via process parameters. Results highlight the combined role of pellet temperature and die residence time in optimizing pellet durability while lowering specific energy use (J/kg). Validation with experiments and literature confirms that this framework offers practical guidance to enhance efficiency and sustainability of pelleting. By providing operational parameters to control bonding and energy input, this work supports a more circular economy through efficient conversion of diverse biomass streams into valuable products while reducing energy consumption and greenhouse gas emissions.

cond-mat.soft

Paste extrusion generates a surface lubrication layer

Dense particle-fluid mixtures, or \emph{pastes}, are encountered in the production of various materials, including animal feed, human food, pharmaceuticals, and biomass for bioenergy. The flow behavior of such dense deformable particulate media is poorly understood, as the interplay between applied stresses, particle deformability and interstitial fluids can be very complex. One challenging context is high pressure pipe flow, encountered in extrusion. Despite its widespread use, many questions remain about how during high pressure flow of the paste, the particle-fluid mixture behaves and interacts with boundaries. We show how high pressure paste extrusion induces the formation of a fluid boundary thinner than the particle size. The induced fluid layer emerges from a pressure-induced phase segregation process. The fluid layer is sufficiently thin to affect particle-wall contacts, making the paste friction coefficient tunable. Our results so offer potential pathways for reducing energy consumption and even extrusion product composition and failure.

cond-mat.soft