arXiv subjects

Raquel Rodriguez-Lamas

Publications and source records attributed to Raquel Rodriguez-Lamas.

3 recordsLinked to original sources

arXiv2026

Multilayer Laue Lenses for Enhanced Spatial Resolution in Dark-Field X-ray Microscopy

We introduce the use of a crossed pair of Multilayer Laue Lenses (MLLs) as an objective in Dark-Field X-ray Microscopy (DFXM). In a demonstration experiment at the ID03 beamline at ESRF, two flat Mo-Si MLLs were used, with a physical aperture of 50 x 50 $\mathrm{\mu m^2}$ and a focal length of 14.25 mm at 19 keV. Applying a 10 % criterion to the Modulation Transfer Functions (MTFs) acquired, a spatial resolution of 56 nm is obtained in bright-field mode -- more than three times better than with a compound refractive lens (CRL) objective. The dark-field resolution is similar. With an efficiency of 26.7 % the MLL objective expands the science domain of DFXM significantly, both for bulk and near-surface studies. Similar to the CRL case, the reciprocal space resolution is dominated by the numerical aperture (NA) of the objective, with the NA being three times larger in the MLL case. This enables faster orientation mapping and implies improved options for the use of tomographic reconstruction algorithms. Although the MLL objective pupil varies with energy and position, secondary peaks are suppressed, simplifying both interpretation and forward simulations. We present an example DFXM application using the MLL as an objective, imaging a through-silicon via Kelvin device.

cond-mat.mtrl-sci↗

arXiv2026

Revealing Dislocation Interactions Controlling Mechanical Properties of Metals

During plastic deformation, metals change shape while continuously becoming stronger. The microscopic origin of these processes lies in the proliferation and movement of line defects, dislocations, and the subsequent self-organisation and pinning of dislocations on lattice imperfections, including other dislocations. The nature of these multiscale processes has remained elusive because in situ observations have not been feasible. We present 3D movies of how dislocations pile up near an obstacle, deeply within a mm-sized pure Al sample and during tensile deformation. Cross-slip is found to provide a mechanism for the dislocations to escape the pile-up, leading to pronounced intermittent behaviour. Such data support a new generation of dislocation dynamics and micro-mechanics modelling.

cond-mat.mtrl-sci↗

arXiv2023

3D Microstructural and Strain Evolution During the Early Stages of Tensile Deformation

Dislocation patterning and self-organization during plastic deformation are associated with work hardening, but the exact mechanisms remain elusive. This is partly because studies of the structure and local strain during the initial stages of plastic deformation has been a challenge. Here we use Dark Field X-ray Microscopy to generate 3D maps of embedded $350 \times 900 \times 72 \,μ\mathrm{m}^3$ volumes within three pure Al single crystals, all oriented for double slip on the primary and conjugate slip systems. These were tensile deformed by 0.6$\%$, 1.7$\%$ and 3.6$\%$, respectively. Orientation maps revealed the existence of two distinct types of planar dislocation boundaries both at 0.6$\%$ and 1.7$\%$ but no systematic patterning. At 3.6$\%$, these boundaries have evolved into a well-defined checkerboard pattern, characteristic of Geometrically Necessary Boundaries, GNBs. The GNB spacing is $\approx$ 14 $μ$m and the misorientation $\approx$ 0.2°, in fair agreement with those at higher strains. By contrast to the sharp boundaries observed at higher strains, the boundaries are associated with a sinusoidal orientation gradient. Maps of the elastic strain along the (111) direction exhibit fluctuations of $\pm 0.0002 $ with an average domain size of 3 $μ$m.

cond-mat.mtrl-sci↗