arXiv subjects

S. Katrych

Publications and source records attributed to S. Katrych.

40 records · Page 3Linked to original sources

arXiv2008

Single crystal of superconducting SmFeAsO1-xFy grown at high pressure

Single crystals of SmFeAsO1-xFy of a size up to 120 micrometers have been grown from NaCl/KCl flux at a pressure of 30 kbar and temperature of 1350-1450 C using the cubic anvil high-pressure technique. The superconducting transition temperature of the obtained single crystals varies between 45 and 53 K.Obtained crystals are characterized by a full diamagnetic response in low magnetic fields and by a high critical current density in high magnetic fields. Structural refinement has been performed on single crystal. Differential thermal analysis investigations at 1 bar Ar pressure show decomposition of SmFeAsO1-xFy at 1302 C.

cond-mat.supr-con↗

arXiv2008

Magnetic penetration depth of single crystal SmFeAsO_{1-x}F_y: a fully gapped superconducting state

We report measurements of the in-plane magnetic penetration depth $λ$ in single crystals of SmFeAsO$_{1-x}$F$_y$ ($x\simeq y \simeq 0.2$) with $T_c \simeq 45$ K. We find that at low temperature $λ$ has an exponential temperature dependence which suggests that the Fermi surface is fully gapped. The magnitude of the minimum energy gap, $Δ_1=1.1\pm 0.1 k_BT_c$ at T=0 K, is significantly smaller than the BCS weak-coupling value suggesting that the gap is either strongly anisotropic or varies significantly between the different Fermi surface sheets. Our data fits well a two gap model with an additional larger gap of magnitude $Δ_2 = 1.8\pm0.2 k_BT_c$ which is associated with $\sim 80$% of the total superfluid density.

cond-mat.supr-con↗

arXiv2007

Synthesis and Bulk Properties of Oxychloride Superconductor Ca2-xNaxCuO2Cl2

Polycrystalline samples and submillimeter size single crystals of Na-doped Ca2CuO2Cl2 have been synthesized under high pressure. A series of experiments showed that the Na content depends not only on the pressure during the synthesis but also on the synthesis temperature and time. From a comparison of the Na-CCOC data with those of structurally related La214 cuprate superconductors we concluded that chlorine at the apical site is less effective that oxygen in supplying charge carriers to the CuO2 plans. As a result, the coupling between the CuO2 planes is weakened, the transition temperature Tc is reduced and the anisotropic nature is enhanced.

cond-mat.supr-con↗

arXiv2007

MgB2 single crystals substituted with Li and with Li-C: Structural and superconducting properties

The effect of Li substitution for Mg and of Li-C co-substitution on the superconducting properties and crystal structure of MgB2 single crystals has been investigated. It has been found that hole doping with Li decreases the superconducting transition temperature Tc, but at a slower rate than electron doping with C or Al. Tc of MgB2 crystals with simultaneously substituted Li for Mg and C for B decreases more than in the case where C is substituted alone. This means that holes introduced by Li cannot counterbalance the effect of decrease of Tc caused by introduction of electrons coming from C. The possible reason of it can be that holes coming from Li occupy the pi band while electrons coming from C fill the sigma band. The temperature dependences of the upper critical field Hc2 for Al and Li substituted crystals with the same Tc show a similar dHc2/dT slope at Tc and a similar Hc2(T) behavior, despite of much different substitution level. This indicates that the mechanism controlling Hc2 and Tc is similar in both hole and electron doped crystals. Electrical transport measurements show an increase of resistivity both in Li substituted crystals and in Li and C co-substituted crystals. This indicates enhanced scattering due to defects introduced by substitutions including distortion of the lattice. The observed behavior can be explained as a result of two effects, influencing both Tc and Hc2. The first one is doping related to the changes in the carrier concentration, which may lead to the decrease or to the increase of Tc. The second one is related to the introduction of new scattering centers leading to the modification of the interband and/or intraband scattering and therefore, to changes in the superconducting gaps and to the reduction of Tc.

cond-mat.supr-con↗