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Shuji Kamegaki

Publications and source records attributed to Shuji Kamegaki.

3 recordsLinked to original sources

High Entropy Alloy under Shock Compression: Optical-Pump X-Ray-Probe

High entropy alloys (HEAs) are multi-principal-element alloys designed for tailorable mechanical performance and have been attracting significant engineering interest, yet their fundamental behaviour under extreme dynamic conditions, such as shock loading, remains unexplored. Here, we report laser-shock experiments on two different types of 1-micrometers-thick HEA microfilms, CuPdAgPtAu and CrFeCoNiCuMo, on 25-micrometers-thick black-Kapton ablator driven by a high intensity laser pulse (532 nm, 5 ns, 16 J, 0.5-mm diameter focal spot) and probed by an X-ray free electron laser (XFEL) pulse (12 keV, 7 fs). Time-resolved X-ray diffraction (XRD) shows the formation of a transient phase with a lattice compression up to 5.1% of the CuPdAgPtAu HEA along the (111) plane; this transient compressed phase existed for 0.3 ns. The impedance matching Hugoniot analysis estimated a shock pressure of 55 +/- 6 GPa in the HEA film, while Au- and Fe-based equations of state (EoS) modelling predict 80 GPa (0.8 MBar) at the free HEA surface. The free HEA surface reached maximum velocities of ~ 5 km/s as recorded from in situ monitoring with the velocity interferometry system for any reflector (VISAR) imaging. These initial HEA results show the suitability of HEA sample preparation and XFEL-based XRD characterisation under extreme shock loading, and are promising for experimental determination of the EoS of this emerging class of materials (beamtime proposal No.: 2024A8503 for a 6-hour preliminary experiment).

cond-mat.mtrl-sci

Structure orientation determined in transmission and reflection: q-plate

Determination of orientation in the imaged sample/scene has a large application potential when the anisotropy of properties is analysed, usually, under a linearly polarised illumination. This study combined several improvements of microscopy imaging: use of an incoherent white illumination source (a lamp) with a spectral filter to define a spectral window, a plastic circular polariser to image with circularly polarised light (instead of linear), and a 4-pol. camera with integrated polarisers for simultaneous acquisition of images at four pi/4-azimuth shifts. In the transmission mode, a high-fidelity readout of form birefringent optical elements, q-plates, was achieved using a fitting procedure based on the analytical expression of S0 (intensity) Stokes parameters at the pixel level. In the reflection mode, the S0 fit was used to determine the azimuth orientation of the q-plates, as well as a generic Amp x cos(2Q1 - 2Q0) + Offset fit (at pixel level) applied to images taken at four Q1 azimuths. The 4-pol. analysis in reflection under circularly polarised illumination is discussed.

physics.optics

Determination of Stokes vector from a single image acquisition

Four Stokes parameters (1852) define the polarisation state of light. Measured changes of the Stokes vector of light traversing an inhomogeneous sample are linked to the local anisotropies of absorption and refraction and are harnessed over an increasing range of applications in photonics, material, and space/earth observation. Several independent polarisation sensitive measurements are usually required for determination of the all four Stokes parameters, which makes such characterisation procedure time-consuming or requires complex setups. Here we introduce a single-snapshot approach to Stokes polarimetry in transmission by use of a 4-polarisation camera with the on-chip integrated polarisers. A quarter-waveplate was added in front of the sample and was illuminated by a linearly polarised light. This approach is demonstrated by measuring birefringence $Δn\sim 0.012$ of spider silk of only $\sim 6~μ$m-diameter using microscopy, however, due to its generic nature, it is transferable to other spectral ranges and imaging applications, e.g., imaging from a fast moving satellite or drone or monitoring fast changing events such as phase transitions.

physics.optics