arXiv subjects

Volker Neu

Publications and source records attributed to Volker Neu.

9 recordsLinked to original sources

arXiv2026

Geometric dependence of exchange bias in tilted three-dimensional CoFe/IrMn microwires

The exchange bias (EB) effect, arising from interfacial coupling between ferromagnetic (FM) and antiferromagnetic (AF) layers, induces a unidirectional magnetic anisotropy and underpins a wide range of spintronic functionalities. Extending the EB effect to three-dimensional (3D) architectures enables investigation of interfacial coupling in non-planar structures, which is a key step toward realizing spintronic functionalities beyond planar systems. Achieving this requires the fabrication of FM/AF bilayers with smooth interfaces and well-defined thicknesses on non-planar scaffolds, together with suitable characterization methods. In this work, we realize exchange-biased 3D FM/AF microwires by combining two-photon lithography with magnetron sputtering. CoFe/IrMn bilayers are deposited on microwire scaffolds with inclination angles of 0 deg, 30 deg, 45 deg relative to the substrate, and their magnetization reversal is probed using dark-field magneto-optical Kerr effect (DF-MOKE) magnetometry. We find that the EB and coercive fields vary in a characteristic way with the inclination angle, consistent with the systematic reduction in film thickness expected from inclined directional deposition. In addition, the EB magnitude is influenced by the combined effects of surface roughness of non-planar geometries and the directional growth of the bilayer, highlighting the importance of 3D scaffold surface quality for integrating magnetic multilayers. These results provide insight into the growth and magnetic behavior of sputter-deposited magnetic multilayers with functional interfaces on 3D geometries.

cond-mat.mtrl-sci↗

arXiv2021

Quantum calibrated magnetic force microscopy

We report the quantum calibration of a magnetic force microscope (MFM) by measuring the two-dimensional magnetic stray field distribution of the MFM tip using a single nitrogen vacancy (NV) center in diamond. From the measured stray field distribution and the mechanical properties of the cantilever a calibration function is derived allowing to convert MFM images to quantum calibrated stray field maps. This novel approach overcomes limitations of prior MFM calibration schemes and allows quantum calibrated nanoscale stray field measurements in a field range inaccessible to scanning NV magnetometry. Quantum calibrated measurements of a stray field reference sample allow its use as a transfer standard, opening the road towards fast and easily accessible quantum traceable calibrations of virtually any MFM.

cond-mat.mes-hall↗

arXiv2019

Uncertainty Analysis of Stray Field Measurements by Quantitative Magnetic Force Microscopy

Magnetic force microscopy (MFM) measurements generally provide phase images which represent the signature of domain structures on the surface of nanomaterials. To quantitatively determine magnetic stray fields based on an MFM image requires calibrated properties of the magnetic tip. In this work, an approach is presented for calibrating a magnetic tip using a Co/Pt multilayered film as a reference sample which shows stable well-known magnetic properties and well-defined perpendicular band domains. The approach is based on a regularized deconvolution process in Fourier domain with a Wiener filter and the L-curve method for determining a suitable regularization parameter to get a physically reasonable result. The calibrated tip is applied for a traceable quantitative determination of the stray fields of a test sample which has a patial frequency spectrum covered by that of the reference sample. According to the "Guide to the expression of uncertainty in measurement", uncertainties of the processing algorithm are estimated considering the fact that the regularization influences significantly the quantitative analysis. We discuss relevant uncertainty components and their propagations between real domain and Fourier domain for both, the tip calibration procedure and the stray field calculation, and propose an uncertainty evaluation procedure for quantitative magnetic force microscopy.

physics.data-an↗

arXiv2018

Calibration of multi-layered probes with low/high magnetic moments

We present a comprehensive method for visualisation and quantification of the magnetic stray field of magnetic force microscopy (MFM) probes, applied to the particular case of custom-made multi-layered probes with controllable high/low magnetic moment states. The probes consist of two decoupled magnetic layers separated by a non-magnetic interlayer, which results in four stable magnetic states: +/-ferromagnetic (FM) and +/-antiferromagnetic (A-FM). Direct visualisation of the stray field surrounding the probe apex using electron holography convincingly demonstrates a striking difference in the spatial distribution and strength of the magnetic flux in FM and A-FM states. In situ MFM studies of reference samples are used to determine the probe switching fields and spatial resolution. Furthermore, quantitative values of the probe magnetic moments are obtained by determining their real space tip transfer function (RSTTF). We also map the local Hall voltage in graphene Hall nanosensors induced by the probes in different states. The measured transport properties of nanosensors and RSTTF outcomes are introduced as an input in a numerical model of Hall devices to verify the probe magnetic moments. The modelling results fully match the experimental measurements, outlining an all-inclusive method for the calibration of complex magnetic probes with a controllable low/high magnetic moment.

physics.app-ph↗

arXiv2017

High precision half-life measurement of $^{147}$Sm $α$ decay from thin-film sources

An investigation of the α-decay of $^{147}$Sm was performed using an ultra low-background Twin Frisch-Grid Ionisation Chamber (TF-GIC). Four natural samarium samples were produced using pulsed laser deposition in ultra high vacuum. The abundance of the $^{147}$Sm isotope was mea- sured using inductively coupled plasma mass spectrometry. A combined half-life value for 147Sm of $1.079(26)\times{}10^{11}$ years was measured. A search for the α-decay into the first excited state of $^{143}$Nd has been performed using $γ$-spectroscopy, resulting in a lower half-life limit of $T_{1/2} > 3.1 \times{}10^{18}$ years (at 90% C.L.).

nucl-ex↗

arXiv2015

A new look on the two-dimensional Ising model: thermal artificial spins

We present a direct experimental investigation of the thermal ordering in an artificial analogue of an asymmetric two dimensional Ising system composed of a rectangular array of nano-fabricated magnetostatically interacting islands. During fabrication and below a critical thickness of the magnetic material the islands are thermally fluctuating and thus the system is able to explore its phase space. Above the critical thickness the islands freeze-in resulting in an arrested thermalized state for the array. Determining the magnetic state of the array we demonstrate a genuine artificial two-dimensional Ising system which can be analyzed in the context of nearest neighbour interactions.

cond-mat.mes-hall↗

arXiv2013

Magnetic domain pattern in hierarchically twinned epitaxial Ni-Mn-Ga films

Magnetic shape memory alloys exhibit a hierarchically twinned microstructure, which has been well examined in epitaxial Ni-Mn-Ga films. Here we analyze consequences of this twin within twins microstructure on the magnetic domain pattern. Atomic and magnetic force microscopy are used to probe the correlation between the martensitic microstructure and magnetic domains. We examine consequences of different twin boundary orientations with respect to the substrate normal as well as variant boundaries between differently aligned twinned laminates. A detailed micromagnetic analysis is given which describes the influence of the finite film thickness on the formation of magnetic band domains in these multiferroic materials.

cond-mat.mtrl-sci↗

arXiv2012

Magnetic domain structure of epitaxial Ni-Mn-Ga films

For the magnetic shape memory effect, knowledge about the interaction between martensitic and magnetic domain structure is essential. In the case of Ni-Mn-Ga bulk material and foils, a staircase-like magnetic domain structure with 90{\deg}- and 180{\deg}-domain walls is known for modulated martensite. In the present paper we show that the magnetic domain pattern of thin epitaxial films is fundamentally different. Here we analyze epitaxial Ni-Mn-Ga films by atomic and magnetic force microscopy to investigate the correlation between the twinned martensitic variants and the magnetic stripe domains. The observed band-like domains with partially perpendicular outof-plane magnetization run perpendicular to the microstructure domains defined by twinning variants. These features can be explained by the finite film thickness, resulting in an equilibrium twinning period much smaller than the domain period. This does not allow the formation of a staircase domain patter. Instead the energies of the magnetic and martensitic microstructures are minimized independently by aligning both patterns perpendicularly to each other. By analyzing a thickness series we can show that the observed magnetic domain pattern can be quantitatively described by an adapted band domain model of Kittel.

cond-mat.mtrl-sci↗

arXiv2008

Domain structure of epitaxial Co films with perpendicular anisotropy

Epitaxial hcp Cobalt films with pronounced c-axis texture have been prepared by pulsed lased deposition (PLD) either directly onto Al2O3 (0001) single crystal substrates or with an intermediate Ruthenium buffer layer. The crystal structure and epitaxial growth relation was studied by XRD, pole figure measurements and reciprocal space mapping. Detailed VSM analysis shows that the perpendicular anisotropy of these highly textured Co films reaches the magnetocrystalline anisotropy of hcp-Co single crystal material. Films were prepared with thickness t of 20 nm < t < 100 nm to study the crossover from in-plane magnetization to out-of-plane magnetization in detail. The analysis of the periodic domain pattern observed by magnetic force microscopy allows to determine the critical minimum thickness below which the domains adopt a pure in-plane orientation. Above the critical thickness the width of the stripe domains is evaluated as a function of the film thickness and compared with domain theory. Especially the discrepancies at smallest film thicknesses show that the system is in an intermediate state between in-plane and out-of-plane domains, which is not described by existing analytical domain models.

cond-mat.mtrl-sci↗