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Yuanbo T. Tang

Publications and source records attributed to Yuanbo T. Tang.

6 recordsLinked to original sources

Direct current thermo-mechanical testing: Principles, uncertainty hierarchy, and its role in advanced materials characterisation

Direct current thermo-mechanical testing (DC-TMT), based on resistive Joule heating, enables rapid heating and cooling, steep thermal gradients and simultaneous mechanical loading, making it a powerful tool for probing deformation, phase transformations, oxidation-assisted damage and creep under conditions inaccessible to conventional furnace-based methods. Despite its growing use, DC-TMT lacks formal standardisation and is often misinterpreted as equivalent to bulk isothermal testing, overlooking intrinsic differences in thermal and mechanical fields. This review addresses that gap by consolidating four decades of research on specimen geometry, temperature measurement, strain characterisation and environmental control, and by classifying uncertainty sources as dominant, secondary and conditional. Evidence from modelling and experiment shows that temperature gradients, heating rate and gauge representativeness govern the reliability of inferred material behaviour. Applications across aluminium, steels, nickel-based superalloys, titanium alloys, hardmetals, zirconium alloys, shape memory alloys and additively manufactured systems are critically assessed. The review highlights domains where DC-TMT provides reproducible mechanistic insight and conditions where direct equivalence with bulk data is not warranted. Implications include the need for transparent reporting, multi-sensor temperature validation and integration with electro-thermal modelling to enable rigorous, mechanism-focused interpretation.

cond-mat.mtrl-sci↗

Revealing 3D Strain and Carbide Architectures in Additively Manufactured Ni Superalloys

Fast directional solidification during Laser Additive Manufacturing (LAM) produces a complex microstructure in nickel-based superalloys, comprising columnar grains with cellular sub-grain structures and carbides. Using non-destructive Scanning 3D X-ray Diffraction (S3DXRD), we reveal spatially complex orientation and intergranular strain relationships that couple strongly to processing-induced cellular sub-grain networks and a primary cubic metal carbide (MC) phase. We have examined 3D orientation and elastic strain tensor fields across 82 $γ$ grains together with the spatial distribution of over 37,000 MC carbides in an ABD-900AM alloy sample manufactured by the Directed Energy Deposition (DED) LAM process. Carbides are spatially associated with the cellular sub-grain network with a weak but present orientation relationship with their parent $γ$ grains. The MC carbides, known to be Ti, Ta and Nb rich, form in regions of high solute segregation, resulting in a significant volumetric lattice parameter patterning in the associated $γ$ phase regions. These chemically distinct solute-rich regions possess a higher associated elastic modulus compared to intercellular regions and determine the local residual stress patterning. These results provide the first non-destructive 3D study of the relationship between rapid solidification-induced segregation, deformation heterogeneity and carbide architectures in an additively manufactured Ni-based superalloy. The insights provide crucial detail to rationalise LAM process parameter optimisation and the coupled spatially governed structural performance.

cond-mat.mtrl-sci↗

A New Class of Alumina-Forming Superalloy for 3D Printing

A new class of crack-resistant nickel-based superalloy containing high $γ^\prime$ fraction is studied for the laser-powder bed fusion (L-PBF) process. The effects of the (Nb+Ta)/Al ratio is emphasised, a strategy that is shown to confer excellent low-temperature strength whilst maintaining oxidation resistance at high temperatures via stable alumina scale formation. The processability of the new alloys is characterised with respect to defect assessment by micro-focus x-ray computed tomography; use is made of a prototype turbine blade geometry and the heritage alloy CM247LC as a benchmark. In all cases, some processing-related porosity is present in thin wall sections such as the trailing edge, but this can be avoided by judicious processing. The cracking seen in CM247LC -- in solid-state, liquation and solidification forms -- is avoided. A novel sub-solvus heat treatment strategy is proposed which takes advantage of AM not requiring solutioning; super-solvus heat treatment is inappropriate since it embrittles the material by deterioration of the texture and coarsening of grain boundary carbides. The tensile strength of the new superalloy is greatest when the Nb+Ta content is highest and exceeds that of CM247LC up to $\sim$900$\,$$^\circ$C. The oxidation resistance is best when Al content is highest, and oxidation-assisted cracking resistance maximized when the (Nb+Ta)/Al ratio is balanced. In all cases these are equivalent or superior to that of CM247LC. Nevertheless, the creep resistance of the new alloys is somewhat inferior to that of CM247LC for which the $γ^\prime$, C, and B contents are higher; this implies a processing/property trade-off which requires further clarification.

cond-mat.mtrl-sci↗

On the influence of alloy composition on the additive manufacturability of Ni-based superalloys

The susceptibility of nickel-based superalloys to processing-induced crack formation during laser powder-bed additive manufacturing is studied. Twelve different alloys -- some of existing (heritage) type but also other newly-designed ones -- are considered. A strong inter-dependence of alloy composition and processability is demonstrated. Stereological procedures are developed to enable the two dominant defect types found -- solidification cracks and solid-state ductility dip cracks -- to be distinguished and quantified. Differential scanning calorimetry, creep stress relaxation tests at 1000$^\circ$C and measurements of tensile ductility at 800$^\circ$C are used to interpret the effects of alloy composition. A model for solid-state cracking is proposed, based on an incapacity to relax the thermal stress arising from constrained differential thermal contraction; its development is supported by experimental measurements using a constrained bar cooling test. A modified solidification cracking criterion is proposed based upon solidification range but including also a contribution from the stress relaxation effect. This work provides fundamental insights into the role of composition on the additive manufacturability of these materials.

cond-mat.mtrl-sci↗

Ultra high-temperature deformation in a single crystal superalloy: Meso-scale process simulation and micro-mechanisms

A mesoscale study of a single crystal nickel-base superalloy subjected to an industrially relevant process simulation has revealed the complex interplay between microstructural development and the micromechanical behaviour. As sample gauge volumes were smaller than the length scale of the highly cored structure of the parent material from which they were produced, their subtle composition differences gave rise to differing work hardening rates, influenced by varying secondary dendrite arm spacings, gamma-prime phase solvus temperatures and a topologically inverted gamma/gamma-prime microstructure. The gamma-prime precipitates possessed a characteristic `X' morphology, resulting from the simultaneously active solute transport mechanisms of thermally favoured octodendritic growth and N-type rafting, indicating creep-type mechanisms were prevalent. High resolution-electron backscatter diffraction (HR-EBSD) characterisation reveals deformation patterning that follows the gamma/gamma-prime microstructure, with high geometrically necessary dislocation density fields localised to the gamma/gamma-prime interfaces; Orowan looping is evidently the mechanism that mediated plasticity. Examination of the residual elastic stresses indicated the `X' gamma-prime precipitate morphology had significantly enhanced the deformation heterogeneity, resulting in stress states within the gamma channels that favour slip, and that encourage further growth of gamma-prime precipitate protrusions. The combination of such localised plasticity and residual stresses are considered to be critical in the formation of the recrystallisation defect in subsequent post-casting homogenisation heat treatments.

cond-mat.mtrl-sci↗

Grain Boundary Serration in Nickel Alloy Inconel 600: Quantification and Mechanisms

The serration of grain boundaries in Inconel 600 caused by heat treatment is studied systematically. A new method based on Fourier transforms is used to analyse the multiple wave-like character of the serrated grain boundaries. A new metric -- the serration index -- is devised and utilised to quantify the degree of serration and more generally to distinguish objectively between serrated and non-serrated boundaries. By considering the variation of the serration index with processing parameters, a causal relationship between degree of serration and solution treatment/cooling rate is elucidated. Processing maps for the degree of serration are presented. Two distinct formation mechanisms arise which rely upon grain boundary interaction with carbides: (i) Zener-type dragging which hinders grain boundary migration and (ii) a faceted carbide growth-induced serration.

cond-mat.mtrl-sci↗