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arXiv · 2102.10995

Measurement of the miscut angle in the determination of the Si lattice parameter

Carlo P. Sasso·Giovanni Mana·Enrico Massa
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Abstract

The measurement of the angle between the interferometer front mirror and the diffracting planes is a critical aspect of the Si lattice-parameter measurement by combined x-ray and optical interferometry. In addition to being measured off-line by x-ray diffraction, it was checked on-line by transversely moving the analyser crystal and observing the phase shift of the interference fringe. We describe the measurement procedure and give the miscut angle of the $^{28}$Si crystal whose lattice parameter was an essential input-datum for, yesterday, the determination of the Avogadro constant and, today, the kilogram realisation by counting atoms. These data are a kindness to others that might wish to repeat the measurement of the lattice-parameter of this unique crystal.

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Carlo P. Sasso, Giovanni Mana, Enrico Massa. 2021-02-05. Measurement of the miscut angle in the determination of the Si lattice parameter. https://doi.org/10.1088/1681-7575/abef23

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