SearcharxivSearch

arXiv subjects

Abdalrhaman Koko

Publications and source records attributed to Abdalrhaman Koko.

9 recordsLinked to original sources

Direct current thermo-mechanical testing: Principles, uncertainty hierarchy, and its role in advanced materials characterisation

Direct current thermo-mechanical testing (DC-TMT), based on resistive Joule heating, enables rapid heating and cooling, steep thermal gradients and simultaneous mechanical loading, making it a powerful tool for probing deformation, phase transformations, oxidation-assisted damage and creep under conditions inaccessible to conventional furnace-based methods. Despite its growing use, DC-TMT lacks formal standardisation and is often misinterpreted as equivalent to bulk isothermal testing, overlooking intrinsic differences in thermal and mechanical fields. This review addresses that gap by consolidating four decades of research on specimen geometry, temperature measurement, strain characterisation and environmental control, and by classifying uncertainty sources as dominant, secondary and conditional. Evidence from modelling and experiment shows that temperature gradients, heating rate and gauge representativeness govern the reliability of inferred material behaviour. Applications across aluminium, steels, nickel-based superalloys, titanium alloys, hardmetals, zirconium alloys, shape memory alloys and additively manufactured systems are critically assessed. The review highlights domains where DC-TMT provides reproducible mechanistic insight and conditions where direct equivalence with bulk data is not warranted. Implications include the need for transparent reporting, multi-sensor temperature validation and integration with electro-thermal modelling to enable rigorous, mechanism-focused interpretation.

cond-mat.mtrl-sci

On the configurational force associated with blocked slip bands at grain boundaries in α-Ti

Grain boundaries can block slip-band propagation and generate intense local stress and strain fields that influence subsequent deformation and damage initiation in polycrystalline metals. Conventional geometric criteria, such as Schmid factor and slip-transfer parameters, describe crystallographic compatibility but do not quantify the energetic severity of a blocked slip event. Here, we apply a configurational force framework to high-angular-resolution electron backscatter diffraction (HR-EBSD) measurements obtained from a blocked slip band in commercially pure titanium. By evaluating a J-type equivalent domain integral from the measured elastic field, we quantify both the magnitude and directional dependence of the local energetic driving force associated with the stress localisation; thus, providing an energetic descriptor of the tendency for deformation to extend into the neighbouring grain. The results show a marked decoupling between conventional geometric metrics and the configurational force response, indicating that the local stress-localisation geometry strongly influences which crystallographically admissible extension directions in the neighbouring grain are energetically favoured. The framework provides a physically grounded basis for quantifying blocked-slip severity and for motivating future in situ studies aimed at defining a critical transfer threshold for transfer or cracking.

cond-mat.mtrl-sci

In situ elucidation of mechanisms governing crack transition to plasticity arrest

Despite extensive theoretical treatment of short- to long-crack transitions, direct experimental quantification of how elastic and plastic energy contributions evolve at the crack tip during arrest has remained absent. In this study, we present an in situ investigation of crack propagation in cold-worked AA-5052 using high-resolution scanning electron microscopy digital image correlation (SEM-DIC) and electron backscatter diffraction (EBSD). By reconstructing local crack-tip fields from measured displacement data, we extract mode I and II stress intensity factors and both elastic and elastoplastic energy release rates (ΔJE and ΔJp). The results show that microstructure-sensitive cracks propagate in a mixed-mode manner at low driving force and transition to plasticity-dominated and load-aligned crack, arrested as the crack-tip process zone develops and expands multiple grains. This transition is identified through the divergence of elastic and elastoplastic energy measures (ΔJE >= ΔJP), crack-tip blunting, slip-band emission, and the emergence of localised plastic deformation. These findings demonstrate that crack arrest coincides with a measurable transition in crack-tip energy partitioning and with process-zone expansion beyond grain-scale dimensions. The results establish an experimentally measurable energy-partition criterion for crack arrest and demonstrate that fracture regime transition is governed by

cond-mat.mtrl-sci

DIC2Abaqus: Calculating mixed-mode stress intensity factors from 2D and 3D-stereo displacement fields

Integrating experimental data into simulations is crucial for predicting material behaviour, especially in fracture mechanics. Digital Image Correlation (DIC) provides precise displacement measurements, essential for evaluating strain energy release rates and stress intensity factors (SIF) around cracks. Translating DIC data into CAE software like ABAQUS has been challenging. DIC2CAE, a MATLAB-based tool, automates this conversion, enabling accurate simulations. It uses the J-integral method to calculate SIFs and handles complex scenarios without needing specimen geometry or applied loads. DIC2CAE enhances fracture mechanics simulations' reliability, accelerating materials research and development.

cs.CE

In situ characterisation of slip bands behaviour in ferrite under mechanical loading

This study investigates the behaviour of slip bands, terminated mid-grain in the ferrite grains of age-hardened stainless steel, under different conditions to understand their dislocation activity and response to varying loads. The full Nye lattice curvature tensor was measured in situ using high-resolution electron backscatter diffraction (HR-EBSD) to estimate the total geometrically necessary dislocation density and individual mobile and immobile dislocations activity at the slip band scale. We found that slip bands primarily consist of edge dislocations, marked by a 'blooming zone' at its tip, indicating significant shear deformation and loss of mobile dislocations. The blooming zone expands as the load increases while the slip band thickness remains constant. Coupled with the correlation between mobile and immobile dislocations within the loaded slip bands observed in situ, we observed that the dislocation activities at the slip band were mainly from immobile edge dislocations to maintain the geometrical distortion of the slip band.

cond-mat.mtrl-sci

Estimation of fatigue life of TiN coatings using cyclic micro-impact testing

This paper studies the behaviour of a thin titanium nitride (TiN) coating (1.5 um thick) on a tool steel substrate material under dynamic and cyclic impacts through an approach combining experimental testing and computational modelling. Dynamic impact testing was used to investigate the load-dependent dynamic hardness and assess the energy-dissipation capabilities of the coating system. In cyclic impact tests, the materials experienced permanent plastic deformation in each cycle, ultimately leading to coating failure. Chemical analysis identified an interlayer between the coating and the substrate, while cross-sectional analysis revealed the extent of coating damage due to cycling and impact load. A three-dimensional map was constructed, connecting the acceleration load, sensed depth, and cycles to the coating failure, and an empirical equation used to characterize the relationship between the depth and cycles to failure. The computational model examined the traction component distribution during loading and unloading, with a focus on normal and shear tractions. These findings suggested the potential significance of normal traction in the interfacial fatigue failure due to impact.

physics.app-ph

A Computational Method for the Determination of the Elastic Displacement Field using Measured Elastic Deformation Field

A novel approach was derived to compute the elastic displacement field from a measured elastic deformation field (i.e., deformation gradient or strain). The method is based on integrating the deformation field using Finite Element discretisation. Space and displacement fields are approximated using piece-wise interpolation functions. Hence, the full elastic deformation field can be expressed as nodal displacements, the unknowns. The nodal displacements are then obtained using a least square method. The proposed method was applied to the symmetrical (residual) elastic deformation field measured using high (angular) resolution electron backscatter diffraction around a Vickers micro-indenting impression on a (001) mono-Si crystal sample with the integrated out-of-plane surface displacements matched with the impression topography measured using. The (residual) displacement field was used as the boundary conditions to calculate the three-dimensional stress intensity factors (K_(I,II,III)) at the cracks emanating from the indentation.

cond-mat.mtrl-sci

An iterative method for reference pattern selection in high resolution electron backscatter diffraction (HR-EBSD)

For high (angular) resolution electron backscatter diffraction (HR-EBSD), the selection of a reference diffraction pattern (EBSP0) significantly affects the precision of the calculated strain and rotation maps. This effect was demonstrated in plastically deformed body-centred cubic and face-centred cubic ductile metals (ferrite and austenite grains in duplex stainless steel) and brittle single-crystal silicon, which showed that the effect is not only limited to measurement magnitude but also spatial distribution. An empirical relationship was then identified between the cross-correlation parameter and angular error, which was used in an iterative algorithm to identify the optimal reference pattern that maximises the precision of HR-EBSD.

cond-mat.mtrl-sci

HR-EBSD analysis of in situ stable crack growth at the micron scale

Understanding the local fracture resistance of microstructural features. such as brittle inclusions, coatings, and interfaces at the microscale under complex loading conditions is critical for microstructure-informed design of materials. In this study, a novel approach has been formulated to decompose the J-integral evaluation of the elastic energy release rate to the three-dimensional stress intensity factors directly from experimental measurements of the elastic deformation gradient tensors of the crack field by in situ high (angular) resolution electron backscatter diffraction (HR-EBSD). An exemplar study is presented of a quasi-static crack, inclined to the observed surface, propagating on low index {hkl} planes in a (001) single crystal silicon wafer.

cond-mat.mtrl-sci