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Hiroyuki Takeya

Publications and source records attributed to Hiroyuki Takeya.

At least 37 records · Page 2Linked to original sources

Magnetic entropy change of ErAl2 magnetocaloric wires fabricated by a powder-in-tube method

We report the fabrication of ErAl2 magnetocaloric wires by a powder-in-tube method (PIT) and the evaluation of magnetic entropy change through magnetization measurements. The magnetic entropy change of ErAl2 PIT wires exhibits similar behavior to the bulk counterpart, while its magnitude is reduced by the decrease in the volume fraction of ErAl2 due to the surrounding non-magnetic sheaths. We find that another effect reduces the magnetic entropy change of the ErAl2 PIT wires around the Curie temperature, and discuss its possible origin in terms of a correlation between magnetic properties of ErAl2 and mechanical properties of sheath material.

cond-mat.mtrl-sci↗

Pressure-induced superconductivity in layered pnictogen diselenide NdO$_{0.8}$F$_{0.2}$Sb$_{1-x}$Bi$_x$Se$_2$ (x = 0.3 and 0.7)

Polycrystalline samples of layered pnictogen diselenide NdO0.8F0.2Sb1-xBixSe2 (x = 0 to 0.8) were successfully synthesized by solid-state reactions. Electrical resistivity in the synthesized samples was systematically decreased with an increase in Bi content x. Crystal structure analysis using synchrotron X-ray diffraction suggests that insulator to metal transition upon Bi doping correlates with anomalous change in c-axis length and/or corrugation in conducting layer. The emergence of superconductivity under high pressure is demonstrated using diamond anvil cell (DAC) with boron-doped diamond electrodes, for x = 0.3 and 0.7 as the representative samples. For Sb-rich one (x = 0.3), we observed a superconducting transition with Tconset = 5.3 K at 50 GPa, which is the first-ever report of the superconductivity in layered SbCh2-based (Ch: chalcogen) compounds. The Tconset of x = 0.3 increased with increasing pressure and reached 7.9 K at 70.8 GPa, followed by the gradual decrease in Tc up to 90 GPa. For Bi-rich one (x = 0.7), a superconducting transition with Tconset = 5.9 K was observed at 43.5 GPa, which is the almost comparable to that of x = 0.3; besides, upper critical field (Hc2) is evaluated to be ~10 T for x = 0.7, which is higher than that of x = 0.3 (Hc2 = 6.7 T at 50 GPa).

cond-mat.supr-con↗

Direct Patterning of Boron-doped Amorphous Carbon Using Focused Ion Beam-assisted Chemical Vapor Deposition

The deposition of boron-doped amorphous carbon thin films on SiO2 substrate was achieved via a focused ion beam-assisted chemical vapor deposition of triphenyl borane (C18H15B) and triphenyl borate (C18H15BO3). The existence of boron in the deposited film from triphenyl borane, with a precursor temperature of 90 °C, was confirmed by a core level X-ray photoelectron spectroscopy analysis. The film exhibited a semiconducting behavior with a band gap of 285 meV. Although the band gap was decreased to 197 meV after an annealing process, the film was still semiconductor. Additionally, a drastic reduction of the resistance on the deposited film by applying pressures was observed from an in-situ electrical transport measurements using a diamond anvil cell.

cond-mat.mtrl-sci↗

Mask-less Patterning of Gallium-irradiated Superconducting Silicon Using Focused Ion Beam

A direct patterning technique of gallium-irradiated superconducting silicon has been established by focused gallium-ion beam without any mask-based lithography process. The electrical transport measurements for line and square shaped patterns of gallium-irradiated silicon were carried out under self-field and magnetic field up to 7 T. Sharp superconducting transitions were observed in both patterns at temperature of 7 K. The line pattern exhibited a signature of higher onset temperature above 10 K. A critical dose amount to obtain the superconducting gallium-irradiated silicon was investigated by the fabrication of various samples with different doses. This technique can be used as a simple fabrication method for superconducting device.

physics.app-ph↗

Pressure-induced superconductivity in SnSb2Te4

We report the discovery of a new superconductor from phase change materials SnSb2Te4. Single crystals of SnSb2Te4 were grown using a conventional melting-growth method. The sample resistance under pressure was measured using an originally designed diamond anvil cell with boron-doped diamond electrodes. The pressure dependence of the resistance has been measured up to 32.6 GPa. The superconducting transition of SnSb2Te4 appeared at 2.1 K(Tconset) under 8.1 GPa, which was further increased with applied pressure to a maximum onset transition temperature 7.4K under 32.6 GPa.

cond-mat.mtrl-sci↗

Fabrication of Superconducting YBa2Cu4O8 Film via Coprecipitation

We have successfully synthesized the c-axis oriented YBa2Cu4O8 (Y-124) film on a SrTiO3 (1 0 0) substrate via a coprecipitation and a dip-coating method. The precipitations including Y, Ba and Cu ions were obtained using their metal nitrates solution and the aqueous solution of sodium hydroxide and oxalic acid. Superconducting transition of the synthesized film was observed at 64-70 K corresponding to bulk Y-124 in the magnetization and resistance measurement. The developed method is suitable to synthesize superconducting Y-124 films for technological applications.

cond-mat.supr-con↗

Pressure Effect in Bi-2212 and Bi-2223 Cuprate Superconductor

We report the pressure effect in Bi2Sr2Ca2Cu3O10+δ (Bi-2223) single crystal with a small amount of intergrowth of Bi2Sr2CaCu2O8+δ (Bi-2212). Their superconducting transition temperatures Tcs showed a domelike shape as a function of pressure, which showed a good agreement with the general relation between the carrier concentration and Tc. Our experimental results indicate that high pressure can induce effective carrier doping into the multilayered high-Tc cuprate superconductor

cond-mat.supr-con↗

Synthesis of Hg-based cuprate superconductors $HgBa_{2}Ca_{n-1}Cu_{n}O_{2(n+1)+δ}$ by CsCl flux additional method

We have succeeded in the synthesis of Re-doped $HgBa_{2}Ca_{n-1}Cu_{n}O_{2(n+1)+δ}$ quickly by a sealed tube technique with a bit of CsCl flux. Powder X-ray diffraction measurement revealed that the single phases of Re-doped $HgBa_{2}CuO_{4+δ}$ (Hg1201), $HgBa_{2}CaCu_{2}O_{6+δ}$ (Hg1212), and $HgBa_{2}Ca_{2}Cu_{3}O_{8+δ}$ (Hg1223) formed in 4 h. The sample grains exhibited plate-like crystals with the sizes of 20$\times$20$\times$1 $μm^{3}$ and the chemical compositions of Hg1201, Hg1212, and Hg1223. The superconducting transitions were observed at 25 K for Hg1201, 122 for Hg1212, and 133 K for Hg1223 in the magnetic susceptibility. These results indicate that the developed method is useful for the fabrication of Hg-based superconducting wires.

cond-mat.supr-con↗

Data-driven Exploration of Pressure-Induced Superconductivity in AgIn$_{5}$Se$_{8}$

Candidates compounds for new thermoelectric and superconducting materials, which have narrow band gap and flat bands near band edges, were exhaustively searched by a high-throughput first-principles calculation from an inorganic materials database named AtomWork. We focused on AgIn$_{5}$Se$_{8}$ which has high density of state near the Fermi level. AgIn$_{5}$Se$_{8}$ was successfully synthesized as single crystals using a melt and slow cooling method. The single-crystal X-ray diffraction analysis revealed the obtained crystal is high quality without deficiencies. The valence states in AgIn$_{5}$Se$_{8}$ were determined to be Ag1+, In3+ and Se2- in accordance with a formal charge by the core level X-ray photoelectron spectroscopy analysis. The electrical resistance was evaluated under high pressure using a diamond anvil cell with boron-doped diamond electrodes. Although the sample was insulator with a resistance of above 40 MΩ at ambient pressure, the resistance markedly decreased with increase of the pressure, and a pressure-induced superconducting transition was discovered at 3.4 K under 52.5 GPa. The transition temperature increased up to 3.7 K under further pressure of 74.0 GPa.

cond-mat.supr-con↗

Pressure-induced Superconductivity in Tin Sulfide

Tin sulfide (SnS) was successfully synthesized in single crystals by a melt and slow-cooling method. The obtained sample was characterized by an X-ray diffraction, an energy dispersive spectrometry, and an X-ray photoelectron spectroscopy. Electrical transport properties in SnS were investigated under high pressure using a diamond anvil cell with boron-doped metallic diamond electrodes and undoped diamond insulating layer. We successfully observed an insulator to metal transition from 12.5 GPa and pressure-induced superconductivity at 5.8 K under 47.8 GPa as predicted by a theoretical calculation.

cond-mat.supr-con↗

Ionic-liquid-gating setup for stable measurements and reduced electronic inhomogeneity at low temperatures

The ionic-liquid-gating technique can be applied to the search for novel physical phenomena at low temperatures because of its wide controllability of the charge carrier density. Ionic-liquid gated field-effect transistors are often fragile upon cooling, however, because of the large difference between the thermal expansion coefficients of frozen ionic liquids and solid target materials. In this paper, we provide a practical technique for setting up ionic-liquid-gated field-effect transistors for low-temperature measurements. It allows stable measurements and reduces the electronic inhomogeneity by reducing the shear strain generated in frozen ionic liquid.

cond-mat.mtrl-sci↗

Pressure-induced Insulator to Metal Transition of Mixed Valence Compound Ce(O,F)SbS$_{2}$

Transport properties of Ce$_{0.85}$F0.15SbS$_{2}$ and undoped CeOSbS$_{2}$ under high pressure were investigated experimentally and theoretically. Electrical resistivity measurements of the Ce$_{0.85}$F0.15SbS$_{2}$ single crystals were performed under various high pressures using a diamond anvil cell with boron-doped diamond electrodes. The samples showed the insulator to metal transition by applying high pressure up to 30-40 GPa. On the other hand, the undoped CeOSbS$_{2}$ showed almost same transport property with the F-doped sample under high pressure. The valence state analysis using X-ray photoelectron spectroscopy revealed a simple valence state of Ce3+ in Ce$_{0.85}$F0.15SbS$_{2}$ and mixed valence state between Ce3+ and Ce4+ in undoped CeOSbS$_{2}$. The valence fluctuation in Ce carried out the comparable transport nature in the both samples. A band calculation suggests that the undoped CeOSbS$_{2}$ could be metallic under high pressure of 30 GPa in accordance with the experimental results. A superior thermoelectric property of power factor in CeOSbS$_{2}$ was estimated under high pressure around 20 GPa in comparison with that of ambient pressure.

cond-mat.mtrl-sci↗

Single Crystal Growth of Cuprate Superconductor (Lu$_{0.8}$Nd$_{0.2}$)Ba$_2$Cu$_4$O$_8$ by KOH Flux Method

Single crystals of Nd-substituted LuBa$_2$Cu$_4$O$_8$ were successfully grown by the KOH flux method. The single phase of Lu$_{1-x}$Nd$_x$Ba$_2$Cu$_4$O$_8$ [(Lu,Nd)124] formed at $x = 0.2$. The compound crystallized as orthorhombic Ammm structure with lattice constants of a = 3.835(3) Å, b = 3.879(2) Å and c = 27.195(6) Å. Single crystal structural analysis demonstrated that the Nd ion partially occupied the Lu site. The (Lu,Nd)124 exhibited the superconducting transition at ~75 K in the magnetic susceptibility and resistivity. The $T_c$ and the c-axis of the (Lu,Nd)124 corresponded to Tm124. These results indicate that RE124 equivalent to the one composed of single RE element is obtained by combination of two RE elements.

cond-mat.supr-con↗

Data-driven Exploration of New Pressure-induced Superconductivity in PbBi$_2$Te$_4$ with Two Transition Temperatures

Candidates compounds for new thermoelectric and superconducting materials, which have narrow band gap and flat bands near band edges, were exhaustively searched by the high-throughput first-principles calculation from an inorganic materials database named AtomWork. We focused on PbBi$_2$Te$_4$ which has the similar electronic band structure and the same crystal structure with those of a pressure-induced superconductor SnBi2Se4 explored by the same data-driven approach. The PbBi$_2$Te$_4$ was successfully synthesized as single crystals using a melt and slow cooling method. The core level X-ray photoelectron spectroscopy analysis revealed Pb2+, Bi3+ and Te2- valence states in PbBi$_2$Te$_4$. The thermoelectric properties of the PbBi$_2$Te$_4$ sample were measured at ambient pressure and the electrical resistivity was also evaluated under high pressure using a diamond anvil cell with boron-doped diamond electrodes. The resistivity decreased with increase of the pressure, and two pressure-induced superconducting transitions were discovered at 3.4 K under 13.3 GPa and at 8.4 K under 21.7 GPa. The data-driven approach shows promising power to accelerate the discovery of new thermoelectric and superconducting materials.

cond-mat.supr-con↗

Pressure-induced Superconductivity in Sulfur-doped SnSe Single Crystal Using Boron-doped Diamond Electrode-prefabricated Diamond Anvil Cell

Sulfur-doped SnSe single crystal was successfully synthesized using a melt and slow-cooling method. The chemical composition and valence state of the obtained sample were analyzed by X-ray photoelectron spectroscopy. The pressure range of a diamond anvil cell with boron-doped diamond electrodes was upgraded to 104 GPa using nano-polycrystalline diamond anvil to investigate a pressure effect for the sample. Electrical resistivity measurements of sulfur-doped SnSe single crystal showed the insulator-metal-superconductor transition by applying high pressure up to 75.9 GPa.

cond-mat.supr-con↗

Two Pressure-induced Superconducting Transitions in SnBi$_2$Se$_4$ Explored by Data-driven Materials Search: New Approach to Develop Novel Functional Materials Including Thermoelectric and Superconducting Materials

Candidates for new thermoelectric and superconducting materials, which have narrow band gap and flat bands near band edges, were searched by the high-throughput first-principles calculation from an inorganic materials database. The synthesized SnBi$_2$Se$_4$ among the target compounds showed a narrow band gap of 354 meV, and a thermal conductivity of 1 W/Km at ambient pressure. The sample SnBi$_2$Se$_4$ showed a metal-insulator transition at 11.1 GPa, as predicted by a theoretical estimation. Furthermore, the two pressure-induced superconducting transitions were discovered at under 20.2 GPa and 47.3 GPa. The data-driven search is a promising approach to discover new functional materials.

cond-mat.supr-con↗

Lithography-free control of the position of single walled carbon nanotubes on a substrate by focused ion beam induced deposition of catalyst and chemical vapor deposition

We introduce a novel nanofabrication technique to directly deposit catalyst pads for the chemical vapor deposition synthesis of single-walled carbon nanotubes (SWCNTs) at any desired position on a substrate by Gallium focused ion beam (FIB) induced deposition of silicon oxide thin films from the metalorganic Tetraethyl orthosilicate (TEOS) precursor. A high resolution in the positioning of the SWCNTs is naturally achieved as the imaging and deposition by FIB are conducted concurrently in situ at the same selected point on the substrate. This technique has substantial advantages over the current state-of-the-art methods that are based on complex and multistep lithography processes.

physics.app-ph↗

Diamond anvil cell using boron-doped diamond electrodes covered with undoped diamond insulating layer

Diamond anvil cell using boron-doped metallic diamond electrodes covered with undoped diamond insulating layer have been developed for electrical transport measurements under high pressure. These designed diamonds were grown on a bottom diamond anvil via a nanofabrication process combining microwave plasma-assisted chemical vapor deposition and electron beam lithography. The resistance measurements of high quality FeSe superconducting single crystal under high pressure were successfully demonstrated by just putting the sample and gasket on the bottom diamond anvil directly. The superconducting transition temperature of FeSe single crystal was enhanced up to 43 K by applying uniaxial-like pressure.

cond-mat.supr-con↗