Searcharxiv⌕ Search

arXiv subjects

Nicola Viganò

Publications and source records attributed to Nicola Viganò.

4 recordsLinked to original sources

Full-field fluorescence computed tomography (F3CT) using a calibrated virtual cone-beam pinhole geometry

We present F3CT, a synchrotron-based hyperspectral full-field fluorescence computed tomography technique that avoids raster scanning by combining a pinhole aperture with an energy-resolving 2D detector. A virtual cone-beam model and two-stage calibration-reconstruction workflow enable 3D elemental mapping under full-field illumination. The method is demonstrated on biological and geological specimens, resolving silver-stain distributions in zebrafish tissue and high-energy fluorescence signatures in rock cores. Phase-contrast tomograms acquired sequentially under the same experimental geometry provide co-registered structural context. F3CT provides a high-throughput route to 3D XRF imaging and establishes a foundation for correlated structural and chemical tomography, with potential for future in-situ and operando implementations.

physics.ins-det↗

Noise2Ghost: Self-supervised deep convolutional reconstruction for ghost imaging

We present a new self-supervised deep-learning-based Ghost Imaging (GI) reconstruction method, which provides unparalleled reconstruction quality for noisy acquisitions among unsupervised methods. We present the supporting mathematical framework and results from theoretical and real data use cases. Self-supervision removes the need for clean reference data while offering strong noise reduction. This provides the necessary tools for addressing signal-to-noise ratio concerns for GI acquisitions in emerging and cutting-edge low-light GI scenarios. Notable examples include micro- and nano-scale x-ray emission imaging, e.g., x-ray fluorescence imaging of dose-sensitive samples. Their applications include in-vivo and in-operando case studies for biological samples and batteries.

cs.CV↗

Determination of five-parameter grain boundary characteristics in nanocrystalline Ni-W by Scanning Precession Electron Diffraction Tomography

Determining the full five-parameter grain boundary characteristics from experiments is essential for understanding grain boundaries impact on material properties, improving related models, and designing advanced alloys. However, achieving this is generally challenging, in particular at nanoscale, due to their 3D nature. In our study, we successfully determined the grain boundary characteristics of an annealed nickel-tungsten alloy (NiW) nanocrystalline needle-shaped specimen (tip) containing twins using Scanning Precession Electron Diffraction (SPED) Tomography. The presence of annealing twins in this face-centered cubic (fcc) material gives rise to common reflections in the SPED diffraction patterns, which challenges the reconstruction of orientation-specific virtual dark field (VDF) images required for tomographic reconstruction of the 3D grain shapes. To address this, an automated post-processing step identifies and deselects these shared reflections prior to the reconstruction of the VDF images. Combined with appropriate intensity normalization and projection alignment procedures, this approach enables high-fidelity 3D reconstruction of the individual grains contained in the needle-shaped sample volume. To probe the accuracy of the resulting boundary characteristics, the twin boundary surface normal directions were extracted from the 3D voxelated grain boundary map using a 3D Hough transform. For the sub-set of coherent Sigma 3 boundaries, the expected {111} grain boundary plane normals were obtained with an angular error of less than 3{\textdegree} for boundary sizes down to 400 nm${}^2$. This work advances our ability to precisely characterize and understand the complex grain boundaries that govern material properties.

cond-mat.mtrl-sci↗

Synchrotron-based X-ray Fluorescence Ghost Imaging

X-ray Fluorescence Ghost Imaging (XRF-GI) was recently demonstrated for x-ray lab sources. It has the potential to reduce acquisition time and deposited dose by choosing their trade-off with spatial resolution, while alleviating the focusing constraints of the probing beam. Here, we demonstrate the realization of synchrotron-based XRF-GI: We present both an adapted experimental setup and its corresponding required computational technique to process the data. This extends the above-mentioned potential advantages of GI to synchrotron XRF imaging. In addition, it enables new strategies to improve resilience against drifts at all scales, and the study of previously inaccessible samples, such as liquids.

physics.optics↗