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Untethered microbot powered by giant magnetoelastic strain

Magnetic elastomers deform under a magnetic field, working as a soft actuator. Untethered microbot made of magnetic elastomers have great potentials in performing medical tasks inside human body as mini doctors. However, the lack of a highly deformable and efficient actuator strongly limits the development of magnetic microbots. In this paper, we developed an actuator of magnetic elastomer capable of large deformation strain by harnessing magnetic pull-in instability. We design three prototypes of untethered microbots by using this actuator: a robot grips objects with a large rotating angle, a robot navigates in a fluid channel and delivers drug, and a robot self-accelerates and quickly jumps up. The pull-in mechanism enables a new type of soft robot with fast response, remote wireless control and extremely high power density.

physics.app-ph↗

An Ultrasensitive 3D Printed Tactile Sensor for Soft Robotics

A new method is presented to manufacture piezoresistive tactile sensors using fused deposition modelling (FDM)printing technology with two different filaments made of thermoplastic polyurethane (TPU) and polylactic acid-graphene (PLA-G) composite. The sensor shows very high sensitivity (gauge factor~550) and excellent recovery to bending-induced strain and can detect a wide range of pressures. This new technology opens the door for 3D printing soft robotic parts capable of tactile communications.

physics.app-ph↗

Beam-controlled spectral-selective architecture with planar polydimethylsiloxane/metal-films for all-day radiative cooling

Radiative cooling is a passive cooling strategy with zero consumption of electricity. Although this technology can work well during optimal atmospheric conditions at nighttime, it is essential to achieve efficient radiative cooling during daytime when peak cooling demand actually occurs. In this article, we report an inexpensive planar polydimethylsiloxane (PDMS)/metal thermal emitter, i.e., a thin film structure fabricated using fast solution coating process that is scalable for large area manufacturing. By manipulating the beaming effect of the thermal radiation, temperature reduction of 9.5 °C and 11.0 °C were demonstrated in the laboratory and out-door environment, respectively. In addition, a spectral-selective solar shelter architecture was designed and implemented to suppress the solar input during the daytime. Due to the enhanced directionality of the thermal emission, the dependence of the radiative cooling performance on the surrounding environment was minimized. Out-door experiments were performed in Buffalo NY, realizing continuous all-day radiative cooling with an average power of ~120 W/m2 on a typical clear sunny day at Northern United States latitudes. This practical passive cooling strategy that cools without any electricity input could have a significant impact on global energy consumption.

physics.app-ph↗

Building a Casimir Metrology Platform with a Commercial MEMS Accelerometer

The Casimir Effect is a physical manifestation of quantum fluctuations of the electromagnetic vacuum. When two metal plates are placed closely together, typically much less than a micron, the long wavelength modes between them are frozen out, giving rise to a net attractive force between the plates, scaling as d^-4 (or d^-3 for a spherical-planar geometry) even when they are not electrically charged. In this paper we observe the Casimir Effect in ambient conditions using a modified capacitive MEMS accelerometer. Using a feedback assisted pick-and-place assembly process we are able to attach various micro-structures onto the post-release MEMS, converting it from an inertial force sensor to a direct force measurement platform with pN resolution. With this system we are able to directly measure the Casimir force between a silver-coated microsphere and gold-coated silicon plate. This device is a step towards leveraging the Casimir Effect for cheap, sensitive, room temperature quantum metrology.

physics.app-ph↗

Spatially controlled electrostatic doping in graphene p-i-n junction for hybrid silicon photodiode

Sufficiently large depletion region for photocarrier generation and separation is a key factor for two-dimensional material optoelectronic devices, but few device configurations has been explored for a deterministic control of a space charge region area in graphene with convincing scalability. Here we investigate a graphene-silicon p-i-n photodiode defined in a foundry processed planar photonic crystal waveguide structure, achieving visible - near-infrared, zero-bias and ultrafast photodetection. Graphene is electrically contacting to the wide intrinsic region of silicon and extended to the p an n doped region, functioning as the primary photocarrier conducting channel for electronic gain. Graphene significantly improves the device speed through ultrafast out-of-plane interfacial carrier transfer and the following in-plane built-in electric field assisted carrier collection. More than 50 dB converted signal-to-noise ratio at 40 GHz has been demonstrated under zero bias voltage, with quantum efficiency could be further amplified by hot carrier gain on graphene-i Si interface and avalanche process on graphene-doped Si interface. With the device architecture fully defined by nanomanufactured substrate, this study is the first demonstration of post-fabrication-free two-dimensional material active silicon photonic devices.

physics.app-ph↗

Towards wafer-scale diamond nano- and quantum technologies

We investigate native nitrogen (NV) and silicon vacancy (SiV) color centers in commercially available, heteroepitaxial, wafer-sized, mm thick, single-crystal diamond. We observe single, native NV centers with a density of roughly 1 NV per $μm^3$ and moderate coherence time ($T_2 = 5 μs$) embedded in an ensemble of SiV centers. Low-temperature spectroscopy of the SiV zero phonon line fine structure witnesses high crystalline quality of the diamond especially close to the growth surface, consistent with a reduced dislocation density. Using ion implantation and plasma etching, we verify the possibility to fabricate nanostructures with shallow color centers rendering our diamond material promising for fabrication of nanoscale sensing devices. As this diamond is available in wafer-sizes up to $100 mm$ it offers the opportunity to up-scale diamond-based device fabrication.

cond-mat.mtrl-sci↗

Lightweight Carbon Fiber Mirrors for Solar Concentrator Applications

Lightweight parabolic mirrors for solar concentrators have been fabricated using carbon fiber reinforced polymer (CFRP) and a nanometer scale optical surface smoothing technique. The smoothing technique improved the surface roughness of the CFRP surface from ~3 μm root mean square (RMS) for as-cast to ~5 nm RMS after smoothing. The surfaces were then coated with metal, which retained the sub-wavelength surface roughness, to produce a high-quality specular reflector. The mirrors were tested in an 11x geometrical concentrator configuration and achieved an optical efficiency of 78% under an AM0 solar simulator. With further development, lightweight CFRP mirrors will enable dramatic improvements in the specific power, power per unit mass, achievable for concentrated photovoltaics in space.

physics.app-ph↗

Fiber to Chip Fusion Splicing for Robust, Low Loss Photonic Packaging

Silicon photonic devices are poised to enter high volume markets such as data-communications, telecommunications, biological sensing, and optical phased arrays; however, permanently attaching a fiber to the photonic chip with high optical efficiency remains a challenge. We present a robust and low-loss packaging technique of permanent optical edge coupling between a fiber and a chip using fusion splicing which is low-cost and scalable to high volume manufacturing. We fuse a SMF-28 cleaved fiber to the chip via CO$_2$ laser and reinforce it with optical adhesive. We demonstrate minimum loss of 1.0dB per-facet with 0.6dB penalty over 160nm bandwidth from 1480nm-1640nm.

physics.app-ph↗

Piezoelectric-based uniaxial pressure cell with integrated force and displacement sensors

We present a design for a piezoelectric-driven uniaxial stress cell suitable for use at ambient and cryogenic temperatures, and that incorporates both a displacement and a force sensor. The cell has a diameter of 46 mm and a height of 13 mm. It can apply a zero-load displacement of up to ~45 $μ$m, and a zero-displacement force of up to ~245 N. With combined knowledge of the displacement and force applied to the sample, it can quickly be determined whether the sample and its mounts remain within their elastic limits. In tests on the oxide metal Sr$_2$RuO$_4$, we found that at room temperature serious plastic deformation of the sample onset at a uniaxial stress of ~0.2 GPa, while at 5 K the sample deformation remained elastic up to almost 2 GPa. This result highlights the usefulness of in situ tuning, in which the force can be applied after cooling samples to cryogenic temperatures.

physics.app-ph↗

Scalable Analysis for Arbitrary Photonic Integrated Waveguide Meshes

The advances in fabrication processes in different material platforms employed in integrated optics are opening the path towards the implementation of circuits with increasing degree of complexity. In addition to the more conventional Application Specific Photonic Circuit (ASPIC) paradigm the Programmable Multifunctional Nanophotonics (PMN) approach is a transversal concept inspired by similar approaches, which are already employed in other technology fields. For instance, in electronics Field Programmable Gate Array (FPGA) devices enable a much more flexible universal operation as compared to Application Specific Integrated Circuits (ASICs).In photonics, the (PMN) concept is enabled by two dimensional (2D) waveguide meshes for which, the number of possible input and output ports quickly builds up and furthermore, internal signal flow paths make the computation of transfer functions an intractable problem. Here we report a scalable method based on mathematical induction that allows one to obtain the scattering matrix of any 2D integrated photonic waveguide mesh circuit composed of an arbitrary number of cells and which is easily programmable. To our knowledge this is the first report of the kind and our results open the path to unblock this important design bottleneck.

physics.app-ph↗

Low-loss Lithium Niobate on Insulator (LNOI) Waveguides of a 10 cm-length and a Sub-nanometer Surface Roughness

We develop a technique for realizing lithium niobate on insulator (LNOI) waveguides of a multi-centimeter-length with a propagation loss as low as 0.027 dB/cm. Our technique relies on patterning a chromium (Cr) thin film coated on the top surface of LNOI into a hard mask with a femtosecond laser followed by the chemo-mechanical polishing for structuring the LNOI into the waveguides. The surface roughness on the waveguides is determined to be 0.452 nm with an atomic force microscope (AFM). The approach is compatible with other surface patterning technologies such as optical and electron beam lithographies or laser direct writing, enabling high-throughput manufacturing of large-scale LNOI-based photonic integrated circuits.

physics.app-ph↗

Dynamic response of ferrofluidic deformable mirrors using elastomer membrane and overdrive techniques

Here are presented the experimental results obtained with a ferrofluidic deformable mirror controlled by electro-magnet actuators. Using a step input through a single actuator we obtain a steady-state settling time of 100ms; however, different combinations of overdrive inputs can be used to decrease it to 25ms. Also, a new technique which consists in laying down an elastomer membrane, coated with an aluminum film, on the ferrofluid is discussed. By adding the membrane on the ferrofluid, it further decreases the time response by a factor of 2. Furthermore, the thin aluminum layer improves the reflectivity of the mirror. Finally, using the membrane and the overdrive techniques combined, the time response is improved by a factor of 20. Numerical simulations show that ferrofluidic mirrors using membranes and improved electronics should reach settling times of the order of a millisecond. Presumably even lower settling times could be possible.

physics.app-ph↗

Laws of 4D printing

The main difference between 3D and 4D printed structures is one extra dimension that is smart evolution over time. However, currently, there is no general formula to model and predict this extra dimension. Here, by starting from fundamental concepts, we derive and validate a universal bi-exponential formula that is required to model and predict the fourth D of 4D printed multi-material structures. 4D printing is a new manufacturing paradigm to elaborate stimuli-responsive materials in multi-material structures for advanced manufacturing (and construction) of advanced products (and structures). It conserves the general attributes of 3D printing (such as the elimination of molds, dies, and machining) and further enables the fourth dimension of products and structures to provide intelligent behavior over time. This intelligent behavior is encoded (usually by an inverse mathematical problem) into stimuli-responsive multi-materials during printing and is enabled by stimuli after printing. Here, we delve into the fourth dimension and reveal three general laws that govern the time-dependent shape-shifting behaviors of almost all (photochemical-, photothermal-, solvent-, pH-, moisture-, electrochemical-, electrothermal-, ultrasound-, enzyme-, etc.-responsive) multi-material 4D structures. We demonstrate that two different types of time-constants govern the shape-shifting behavior of almost all the multi-material 4D printed structures over time. Our results starting from the most fundamental concepts and ending with governing equations can serve as general design principles for future research in the 4D printing field, where the time-dependent behaviors should be understood, modeled, and predicted, correctly. Future software and hardware developments in 4D printing can also benefit from these results.

physics.app-ph↗

Experimental Investigation of Programmed State Stability in OxRAM Resistive Memories

Oxide-based Random Access Memory (OxRAM), is part of the larger family of Resistive RAM (RRAM) memories. Generally OxRAM cells consist of a transition metal oxide (typically HfO2, Ta2O5, TiO2) sandwiched between two metal electrodes (typically TiN, TaN, W but also Pt, Ir). This thesis describes the experimental investigation performed on OxRAM memories during a 6-months internship project at imec research institute (Leuven, Belgium). From previous studies, HfO-based OxRAM memories showed good endurance properties (with more than 10e9 write cycles), low operating current (as low as 10 uA), and very fast switching (programming pulses of 100 ns). However, it has been observed that, under low programming current condition, data stability becomes challenging. Therefore, this programming state stability needed further investigation. This thesis addresses the problem of state stability, first, by presenting the equipment and algorithms used to study OxRAM state loss over short time intervals. Secondly, various experiments and tests are performed searching for a key parameter in order to control memory retention. Finally, this work demonstrates that resistance evolution over time is affected by both a determinist drift (logarithmically dependent on time) and a random stochastic fluctuation component. It also demonstrates that this behavior is intrinsic in the nature of the device itself and does not depend on processing issues or variation in the programming conditions. This experimental study proved the intrinsic nature of the program instability phenomena in OxRAM devices, which in turns leads to the ineffectiveness of verify algorithm for low current operation.

cs.ET↗

A frequency-preserving and time-invariant metamaterial-based nonlinear acoustic diode

We present the realization of an acoustic diode or rectifier, exploiting symmetry-breaking nonlinear effects like harmonic generation and wave mixing and the filtering capabilities of metamaterials. The essential difference and advantage compared with previous acoustic diode realizations is that the present is simultaneously a time invariant, frequency preserving and switchable device. This allows its application also as an on-off or amplitude-tuning switch. We evaluate its properties by means of a numerical study and demonstrate its feasibility in a preliminary experimental realization. This work may provide new opportunities for the practical realization of structural components with one-way wave propagation properties.

physics.app-ph↗

Raman Spectroscopy of Diesel and Gasoline Engine-Out Soot Using Different Laser Power

We studied engine-out soot samples collected from a heavy-duty direct-injection diesel engine and a port-fuel injection gasoline spark-ignition engine. The two types of soot samples were characterized using Raman spectroscopy with different laser power. A Matlab program using least-square-method with trust-region-reflective algorithm was developed for curve fitting. We used a DOE (design of experiments) method to avoid local convergence. This method was used for two-band fitting and three-band fitting. The fitting results were used to determine the intensity ratio of D and G Raman bands. We find that high laser power may cause oxidation of soot samples, which gives higher D/G intensity ratio. Diesel soot has consistently higher amorphous/graphitic carbon ratio and thus higher oxidation reactivity, in comparison to gasoline soot, which is revealed by the higher D/G intensity ratio in Raman spectra measured under the same laser power.

physics.app-ph↗

Use of Magnetoresistive Random-Access Memory as Approximate Memory for Training Neural Networks

Hardware neural networks that implement synaptic weights with embedded non-volatile memory, such as spin torque memory (ST-MRAM), are a major lead for low energy artificial intelligence. In this work, we propose an approximate storage approach for their memory. We show that this strategy grants effective control of the bit error rate by modulating the programming pulse amplitude or duration. Accounting for the devices variability issue, we evaluate energy savings, and show how they translate when training a hardware neural network. On an image recognition example, 74% of programming energy can be saved by losing only 1% on the recognition performance.

cs.ET↗

Thermal-driven Flow inside Graphene Channels for Water Desalination

A novel concept of membrane process in thermal-driven system is proposed for water desalination. By means of molecular dynamics simulations, we show fast water transport through graphene galleries at a temperature gradient. Water molecules are driven to migrate through nanometer-wide graphene channels from cold reservoir to hot reservoir by the effect of thermal creep flow. Reducing the interlayer spacing to 6.5 Å, an abrupt escalation occurs in water permeation between angstrom-distance graphene slabs. The change from disordered bulklike water to quasi-square structure have been found under this extremely confined condition. This leads to a transition to subcontinuum transport. Water molecules perform collective diffusion behaviors inside graphene channels. The special transport processes with structure change convert thermal energy into motion without dissipation, resulting in unexpected high water permeability. The thermal-driven system reaches maximum flowrate at temperature variance of 80 K, corresponding to the quantity at pressure difference up to 10^5 bar in commercial reverse osmosis processes and 230 bar in pressure-driven slip flow. Our results also reveal the movement of saline ions influenced by thermophoretic effect, which complement the geometry limitation at greater layer spacing, enhancing the blockage of ions. This finding aims to provide an innovational idea of developing a high-efficiency desalination technology able to utilize various forms of energy.

cond-mat.soft↗